4'-methyl-2',6-di-tert-butylphenyl (2R,3S,4S)-2,5-bis(benzyloxy)-2,4-dimethyl-3-hydroxypentanoates

Base Information

Chemical Name:4'-methyl-2',6-di-tert-butylphenyl (2R,3S,4S)-2,5-bis(benzyloxy)-2,4-dimethyl-3-hydroxypentanoates
CAS No.:92817-91-9
Molecular Formula:C₃₆H₄₈O₅
Molecular Weight:560.774
Hs Code.:

Synonyms:4'-methyl-2',6-di-tert-butylphenyl (2R,3S,4S)-2,5-bis(benzyloxy)-2,4-dimethyl-3-hydroxypentanoates

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Chemical Property of 4'-methyl-2',6-di-tert-butylphenyl (2R,3S,4S)-2,5-bis(benzyloxy)-2,4-dimethyl-3-hydroxypentanoates

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Technology Process of 4'-methyl-2',6-di-tert-butylphenyl (2R,3S,4S)-2,5-bis(benzyloxy)-2,4-dimethyl-3-hydroxypentanoates

There total 3 articles about 4'-methyl-2',6-di-tert-butylphenyl (2R,3S,4S)-2,5-bis(benzyloxy)-2,4-dimethyl-3-hydroxypentanoates which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

: 92817-91-9
4'-methyl-2',6-di-tert-butylphenyl (2R,3S,4S)-2,5-bis(benzyloxy)-2,4-dimethyl-3-hydroxypentanoates

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / 1.5 M n-BuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 3 h; 2.) r.t., overnight

2: LDA

With n-butyllithium; lithium diisopropyl amide; In tetrahydrofuran; hexane;
DOI:10.1021/ja00338a027

Reference yield:

: 56972-68-0
2-benzyloxy-propionyl chloride

: 92817-91-9
4'-methyl-2',6-di-tert-butylphenyl (2R,3S,4S)-2,5-bis(benzyloxy)-2,4-dimethyl-3-hydroxypentanoates

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / 1.5 M n-BuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 3 h; 2.) r.t., overnight

2: LDA

With n-butyllithium; lithium diisopropyl amide; In tetrahydrofuran; hexane;
DOI:10.1021/ja00338a027