(Z)-1-(2-phenyl-2-p-fluorophenylvinyl)-4-fluoro benzene

Base Information

Chemical Name:(Z)-1-(2-phenyl-2-p-fluorophenylvinyl)-4-fluoro benzene
CAS No.:1223047-89-9
Molecular Formula:C₂₀H₁₄F₂
Molecular Weight:292.328
Hs Code.:

Synonyms:(Z)-1-(2-phenyl-2-p-fluorophenylvinyl)-4-fluoro benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1-(2-phenyl-2-p-fluorophenylvinyl)-4-fluoro benzene

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Technology Process of (Z)-1-(2-phenyl-2-p-fluorophenylvinyl)-4-fluoro benzene

There total 6 articles about (Z)-1-(2-phenyl-2-p-fluorophenylvinyl)-4-fluoro benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 5216-31-9
1,2-bis(4-fluorophenyl)acetylene

: 873-55-2
sodium benzenesulfonate

: 1223047-89-9
(Z)-1-(2-phenyl-2-p-fluorophenylvinyl)-4-fluoro benzene

Guidance literature:: With palladium diacetate; trifluoroacetic acid; naphthalene-1,8-diamine; In 1,4-dioxane; water; at 120 ℃; for 24h; stereoselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1039/c3cc43723j

Reference yield: 63.0%

: 5216-31-9
1,2-bis(4-fluorophenyl)acetylene

: 100-58-3
phenylmagnesium bromide

: 1223047-89-9
(Z)-1-(2-phenyl-2-p-fluorophenylvinyl)-4-fluoro benzene

Guidance literature:: 1,2-bis(4-fluorophenyl)acetylene; phenylmagnesium bromide; With nickel(II) chloride hexahydrate; In tetrahydrofuran; toluene; at 60 ℃; for 1h; Inert atmosphere; Schlenk technique;

With water; In tetrahydrofuran; toluene; stereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1039/c3cc45202f

Reference yield: 59.0%

: 5216-31-9
1,2-bis(4-fluorophenyl)acetylene

: 591-51-5
phenyllithium

: 1223047-89-9
(Z)-1-(2-phenyl-2-p-fluorophenylvinyl)-4-fluoro benzene

Guidance literature:: 1,2-bis(4-fluorophenyl)acetylene; With dmap; n-butyllithium; zirconocene dichloride; In tetrahydrofuran; hexane; at 20 ℃; for 1h; Inert atmosphere;

phenyllithium; In tetrahydrofuran; hexane; at 20 ℃; for 12h; stereoselective reaction; Further stages; Inert atmosphere;
DOI:10.3762/bjoc.10.48