2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoic acid methyl ester

Base Information

• Chemical Name: 2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoic acid methyl ester
• CAS No.: 787629-29-2
• Molecular Formula: C₂₅H₃₂N₂O₆
• Molecular Weight: 456.539

Synonyms:2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoic acid methyl ester

Chemical Property of 2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoic acid methyl ester

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of 2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoic acid methyl ester

There total 2 articles about 2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-octyloxybenzoic acid hydrazide (255062-86-3) + 2-methoxyisophthalic acid monomethyl ester (288099-33-2) → 2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoic acid methyl ester (787629-29-2)

Guidance literature:

With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/ja047436p

Reference yield:

2-octyloxybenzoic acid methyl ester (255062-85-2) → 2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoic acid methyl ester (787629-29-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / hydrazine hydrate / methanol / 5 h / 40 °C

2: 88 percent / DCC / CH₂Cl₂ / 3 h / 20 °C

With hydrazine hydrate; dicyclohexyl-carbodiimide; In methanol; dichloromethane;

DOI:10.1021/ja047436p

Reference yield: 94.0%

2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoic acid methyl ester (787629-29-2) → 2-Methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoic acid hydrazide (787629-30-5)

Guidance literature:

With hydrazine hydrate; In methanol; at 40 ℃; for 2h;

DOI:10.1021/ja047436p

upstream raw materials:

2-octyloxybenzoic acid hydrazide

2-methoxyisophthalic acid monomethyl ester

2-octyloxybenzoic acid methyl ester

Downstream raw materials:

2-Methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoic acid hydrazide

5-(N'-{2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoic acid methyl ester

5-(N'-{2-Methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoic acid hydrazide

2-methoxy-3-{N'-[5-(N'-{2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoyl]-hydrazinocarbonyl}-benzoic acid methyl ester

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