2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-nitrophenyl)-3-oxobutanamide

Base Information

• Chemical Name: 2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-nitrophenyl)-3-oxobutanamide
• CAS No.: 1092963-82-0
• Molecular Formula: C₂₄H₂₂N₂O₈
• Molecular Weight: 466.447

Synonyms:2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-nitrophenyl)-3-oxobutanamide

Chemical Property of 2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-nitrophenyl)-3-oxobutanamide

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Technology Process of 2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-nitrophenyl)-3-oxobutanamide

There total 1 articles about 2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-nitrophenyl)-3-oxobutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

2,7-Dimethoxynaphthalene (3469-26-9) + N-(2-nitrophenyl)-3-oxobutanamide (90915-86-9) + manganese triacetate (638-38-0,993-02-2,2180-18-9,15411-95-7,22981-23-3,27004-39-3) → 1-acetyl-1-hydroxy-8-methoxy-3-(2'-nitrophenyl)-1H-benzo[e]indol-2(3H)-one (1092964-04-9) + 2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-nitrophenyl)-3-oxobutanamide (1092963-82-0) + C23H18N2O7

Guidance literature:

With acetic acid; at 70 ℃; for 0.0333333h;

DOI:10.1055/s-2008-1067206

Reference yield: 79.0%

2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-nitrophenyl)-3-oxobutanamide (1092963-82-0) → 5-chloro-8-methoxy-2-methyl-1-(2-nitrophenylcarbamoyl)naphtho[2,1-b]furan (1134953-19-7)

Guidance literature:

With hydrogenchloride; In water; acetic acid; at 20 ℃; for 9h;

DOI:10.3987/COM-08-11515

Reference yield: 64.0%

2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-nitrophenyl)-3-oxobutanamide (1092963-82-0) + ethylene glycol (107-21-1) → 1-hydroxy-8-methoxy-1-(2-methyl-1,3-dioxolan-2-yl)-3-(2-nitrophenyl)-1H-benz[e]indol-2(3H)-one (1134953-47-1)

Guidance literature:

With hydrogenchloride; In water; at 80 ℃; for 3h;

DOI:10.3987/COM-08-11515

upstream raw materials:

2,7-Dimethoxynaphthalene

N-(2-nitrophenyl)-3-oxobutanamide

manganese triacetate

Downstream raw materials:

5-chloro-8-methoxy-2-methyl-1-(2-nitrophenylcarbamoyl)naphtho[2,1-b]furan

1-hydroxy-8-methoxy-1-(2-methyl-1,3-dioxolan-2-yl)-3-(2-nitrophenyl)-1H-benz[e]indol-2(3H)-one

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