Hexanedioic acid 1-butyl ester

Base Information

• Chemical Name: Hexanedioic acid 1-butyl ester
• CAS No.: 7529-33-1
• Molecular Formula: C10H18O4
• Molecular Weight: 202.251
• Mol file: 7529-33-1.mol

Synonyms:Monobutyladipinsaeureester;Adipinsaeure-monobutylester;adipic acid monobutyl ester;Hexanedioic acid monobutyl ester;Monobutyl-adipat;

Chemical Property of Hexanedioic acid 1-butyl ester

Chemical Property:

• Vapor Pressure: 8.87E-05mmHg at 25°C
• Boiling Point: 316.2°C at 760 mmHg
• Flash Point: 117.3°C
• PSA: 63.60000
• Density: 1.054g/cm³
• LogP: 1.97470

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Hexanedioic acid 1-butyl ester

There total 3 articles about Hexanedioic acid 1-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

Adipic acid (124-04-9) + n-butyl formate (592-84-7) → Hexanedioic acid monobutyl ester (7529-33-1) + adipic acid dibutyl ester (105-99-7)

Guidance literature:

With Dowex 50Wx₂; In toluene; at 70 ℃; for 5.66667h;

DOI:10.1039/a902325i

Reference yield: 80.0%

Adipic acid (124-04-9) + butan-1-ol (71-36-3) → Hexanedioic acid monobutyl ester (7529-33-1) + adipic acid dibutyl ester (105-99-7)

Guidance literature:

With iron(III) chloride; choline chloride; toluene-4-sulfonic acid; at 70 - 110 ℃; for 6h;

Reference yield:

1-bromo-butane (109-65-9) + Adipic acid (124-04-9) → Hexanedioic acid monobutyl ester (7529-33-1) + adipic acid dibutyl ester (105-99-7)

Guidance literature:

With sodium hydroxide; Aliquat 336; In toluene; for 24h; Heating;

DOI:10.1016/0040-4020(89)80151-6

upstream raw materials:

Adipic acid

butan-1-ol

1-bromo-butane

n-butyl formate

Downstream raw materials:

Vinyl-butyl-adipat