2-chloro-4-methylbenzyl methanesulfonate

Base Information

• Chemical Name: 2-chloro-4-methylbenzyl methanesulfonate
• CAS No.: 219764-31-5
• Molecular Formula: C₉H₁₁ClO₃S
• Molecular Weight: 234.704

Synonyms:2-chloro-4-methylbenzyl methanesulfonate

Chemical Property of 2-chloro-4-methylbenzyl methanesulfonate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

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Technology Process of 2-chloro-4-methylbenzyl methanesulfonate

There total 1 articles about 2-chloro-4-methylbenzyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(2-chloro-4-methylphenyl)methanol (39652-31-8) + methanesulfonyl chloride (124-63-0) → 2-chloro-4-methylbenzyl methanesulfonate (219764-31-5)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 3h;

DOI:10.1021/acs.jmedchem.1c00432

Reference yield: 93.0%

2-chloro-4-methylbenzyl methanesulfonate (219764-31-5) + tert-butyl 3-hydroxyazetidine-1-carboxylate (141699-55-0) → tert-butyl 3-((2-chloro-4-methylbenzyl)oxy)azetidine-1-carboxylate

Guidance literature:

tert-butyl 3-hydroxyazetidine-1-carboxylate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;

2-chloro-4-methylbenzyl methanesulfonate; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 38h;

DOI:10.1021/acs.jmedchem.1c00432

Reference yield:

2-chloro-4-methylbenzyl methanesulfonate (219764-31-5) + methyl 2-methyl-1H-imidazo[4,5-b]pyridine-5-carboxylate (219763-98-1) → methyl 1-(2-chloro-4-methylbenzyl)-2-methyl-1H-imidazo[4,5-b]pyridine-5-carboxylate + methyl 3-(2-chloro-4-methylbenzyl)-2-methyl-3H-imidazo[4,5-b]pyridine-5-carboxylate

Guidance literature:

upstream raw materials:

(2-chloro-4-methylphenyl)methanol

methanesulfonyl chloride

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