(diethyl phosphoric) 4-methylbenzoic anhydride

Base Information

Chemical Name:(diethyl phosphoric) 4-methylbenzoic anhydride
CAS No.:135580-51-7
Molecular Formula:C₁₂H₁₇O₅P
Molecular Weight:272.238
Hs Code.:

Synonyms:(diethyl phosphoric) 4-methylbenzoic anhydride

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Chemical Property of (diethyl phosphoric) 4-methylbenzoic anhydride

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Technology Process of (diethyl phosphoric) 4-methylbenzoic anhydride

There total 2 articles about (diethyl phosphoric) 4-methylbenzoic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 2117-84-2
diethyl tri-n-butylstannyl phosphate

: 874-60-2
4-methyl-benzoyl chloride

: 135580-51-7
(diethyl phosphoric) 4-methylbenzoic anhydride

Guidance literature:: In tetrachloromethane; Ambient temperature;
DOI:10.1021/ja00533a047

Reference yield: 85.0%

: 814-49-3
diethyl chlorophosphate

: 99-94-5
p-Toluic acid

: 135580-51-7
(diethyl phosphoric) 4-methylbenzoic anhydride

Guidance literature:: With magnesium oxide; at 20 ℃; for 0.333333h;
DOI:10.1081/SCC-120002412

Reference yield: 100.0%

: 135580-51-7
(diethyl phosphoric) 4-methylbenzoic anhydride

: 328249-45-2
(E,E)-4-{4-(3,4,5-tridodecyloxystyryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzaldehyde

: 4-{(E)-2-[4-((E)-2-{2,5-Bis-((S)-2-methyl-butoxy)-4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-2,5-bis-((S)-2-methyl-butoxy)-phenyl]-vinyl}-benzoic acid

Guidance literature:: (diethyl phosphoric) 4-methylbenzoic anhydride; (E,E)-4-{4-(3,4,5-tridodecyloxystyryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzaldehyde; With potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl-formamide;

With potassium hydroxide; In ethanol; at 80 ℃; Further stages.;
DOI:10.1039/b005903j