bis(triphenylstannyl)octamethyltetrasilane

Base Information

Chemical Name:bis(triphenylstannyl)octamethyltetrasilane
CAS No.:210362-77-9
Molecular Formula:C₄₄H₅₄Si₄Sn₂
Molecular Weight:932.675
Hs Code.:

Synonyms:bis(triphenylstannyl)octamethyltetrasilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(triphenylstannyl)octamethyltetrasilane

Chemical Property:

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Technology Process of bis(triphenylstannyl)octamethyltetrasilane

There total 5 articles about bis(triphenylstannyl)octamethyltetrasilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 4774-91-8
1,4-difluorooctamethyltetrasilane

: sodium triphenylstannide

: 210362-77-9
bis(triphenylstannyl)octamethyltetrasilane

Guidance literature:: In tetrahydrofuran; (inert atmosphere); stirring (-40 to -30°C, 2 h), slow warming toroom temp., stirring (4 h); solvent removal (vac., room temp.), addn. of Et2O, filtration, removal of solvent (vac.), recrystn. (Et2O/toluene); elem. anal.;
DOI:10.1515/znb-1999-0217

Reference yield: 68.0%

: 4774-91-8
1,4-difluorooctamethyltetrasilane

: 639-58-7
triphenyltin chloride

: 210362-77-9
bis(triphenylstannyl)octamethyltetrasilane

Guidance literature:: With magnesium; In tetrahydrofuran; byproducts: MgFCl; Schlenk technique, N2; mixt. (Mg excess) stirring for 72 h, THF vac. removal, residue extn. (Et2O), Et2O layer vac. evapn.; residue recrystn. (Et2O/n-hexane); elem. anal.;
DOI:10.1080/10426509708044214

Reference yield:

: 754-75-6
1,4-dichloropermethyltetrasilane

: sodium triphenylstannide

: 210362-77-9
bis(triphenylstannyl)octamethyltetrasilane

: 1064-10-4
hexaphenylditin

Guidance literature:: In tetrahydrofuran; (inert atmosphere); stirring (-40 to -30°C, 2 h), slow warming toroom temp., stirring (4 h); solvent removal (vac., room temp.), addn. of Et2O, filtration, removal of solvent (vac.), recrystn. (Et2O/hexane); elem. anal.;
DOI:10.1515/znb-1999-0217