benzyl tert-butyl (1R,2R)-cyclopentane-1,2-diyldicarbaMate

Base Information

Chemical Name:benzyl tert-butyl (1R,2R)-cyclopentane-1,2-diyldicarbaMate
CAS No.:815645-30-8
Molecular Formula:C₁₈H₂₆N₂O₄
Molecular Weight:334.415
Hs Code.:
Mol file:815645-30-8.mol

Synonyms:tert-butyl (1R,2R)-2-(benzyloxycarbonylamino)cyclopentylcarbamate

Suppliers and Price of benzyl tert-butyl (1R,2R)-cyclopentane-1,2-diyldicarbaMate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Benzyltert-butyl(1R,2R)-cyclopentane-1,2-diyldicarbamate 95+%
1g
$ 772.00

Chemenu
benzyltert-butyl((1R,2R)-cyclopentane-1,2-diyl)dicarbamate 95%
1g
$ 729.00

American Custom Chemicals Corporation
BENZYL TERT-BUTYL-(1R,2R)-CYCLOPENTANE-1,2-DIYLDICARBAMATE 95.00%
1G
$ 1575.00

American Custom Chemicals Corporation
BENZYL TERT-BUTYL-(1R,2R)-CYCLOPENTANE-1,2-DIYLDICARBAMATE 95.00%
5MG
$ 496.60

Alichem
Benzyltert-butyl(1R,2R)-cyclopentane-1,2-diyldicarbamate
1g
$ 684.52

Total 3 raw suppliers

Chemical Property of benzyl tert-butyl (1R,2R)-cyclopentane-1,2-diyldicarbaMate

Chemical Property:

Storage Temp.:2-8°C

Purity/Quality:

≥99% ^*data from raw suppliers

Benzyltert-butyl(1R,2R)-cyclopentane-1,2-diyldicarbamate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of benzyl tert-butyl (1R,2R)-cyclopentane-1,2-diyldicarbaMate

There total 4 articles about benzyl tert-butyl (1R,2R)-cyclopentane-1,2-diyldicarbaMate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: (1R,2R)-2-(tert-butoxycarbonylamino)cyclopentyl isocyanate

: 815645-30-8
tert-butyl (1R,2R)-2-(benzyloxycarbonylamino)cyclopentylcarbamate

Guidance literature:: With copper(l) chloride; In N,N-dimethyl-formamide; at 20 ℃; for 0.75h;
DOI:10.1021/ja046280q

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 815645-30-8
tert-butyl (1R,2R)-2-(benzyloxycarbonylamino)cyclopentylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: Et₃N; ethyl chloroformate / tetrahydrofuran / 0.33 h / 0 °C

1.2: aq. NaN₃ / tetrahydrofuran / 0.33 h / 0 °C

2.1: benzene / 0.5 h / Heating

3.1: CuCl / dimethylformamide / 0.75 h / 20 °C

With chloroformic acid ethyl ester; triethylamine; copper(l) chloride; In tetrahydrofuran; N,N-dimethyl-formamide; benzene; 3.1: Curtius rearrangement;
DOI:10.1021/ja046280q

Reference yield:

: 245115-25-7
(1R,2R)-2-((tert-butoxycarbonyl)amino)cyclopentane-1-carboxylic acid

: 815645-30-8
tert-butyl (1R,2R)-2-(benzyloxycarbonylamino)cyclopentylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: Et₃N; ethyl chloroformate / tetrahydrofuran / 0.33 h / 0 °C

1.2: aq. NaN₃ / tetrahydrofuran / 0.33 h / 0 °C

2.1: benzene / 0.5 h / Heating

3.1: CuCl / dimethylformamide / 0.75 h / 20 °C

With chloroformic acid ethyl ester; triethylamine; copper(l) chloride; In tetrahydrofuran; N,N-dimethyl-formamide; benzene; 2.1: Curtius rearrangement;
DOI:10.1021/ja046280q