[RuH(1,2-bis(dimethylphosphino)ethane)((R)-DIFLUORPHOS)][tetraphenylborate]

Base Information

Chemical Name:[RuH(1,2-bis(dimethylphosphino)ethane)((R)-DIFLUORPHOS)][tetraphenylborate]
CAS No.:1147564-32-6
Molecular Formula:C₂₄H₂₀B*C₄₄H₄₁F₄O₄P₄Ru
Molecular Weight:1254
Hs Code.:

Synonyms:[RuH(1,2-bis(dimethylphosphino)ethane)((R)-DIFLUORPHOS)][tetraphenylborate]

Suppliers and Price of [RuH(1,2-bis(dimethylphosphino)ethane)((R)-DIFLUORPHOS)][tetraphenylborate]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [RuH(1,2-bis(dimethylphosphino)ethane)((R)-DIFLUORPHOS)][tetraphenylborate]

Chemical Property:

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Technology Process of [RuH(1,2-bis(dimethylphosphino)ethane)((R)-DIFLUORPHOS)][tetraphenylborate]

There total 1 articles about [RuH(1,2-bis(dimethylphosphino)ethane)((R)-DIFLUORPHOS)][tetraphenylborate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 55102-19-7
hydridochlorotris(triphenylphosphine)ruthenium(II)

: 503538-69-0,503538-70-3,681259-24-5
(R)-[4,4'-bi(2,2-difluoro-1,3-benzodioxol)-5,5'-diyl]bis(diphenylphosphane)

: 23936-60-9
1,2-bis(dimethylphosphanyl)ethane

: 143-66-8
sodium tetraphenyl borate

: 1147564-32-6
[RuH(1,2-bis(dimethylphosphino)ethane)((R)-DIFLUORPHOS)][tetraphenylborate]

Guidance literature:: In tetrahydrofuran; byproducts: P(C6H5)3, NaCl; (N2, Schlenk technique); heating ruthenium compd., binaphthyl deriv. andTHF at 105°C for 16 h, cooling to room temp., addn. of diphosphi noethane deriv., stirring for 1 h at room temp., addn. of THF soln. of borate salt, stirring for 12 h; filtration through celite, evapn., washing with diethyl ether and benzene, reppn. by slow ether vapour diffusion into satd. THF soln. at room temp., elem. anal.;