trimethyl 1,1'-bis-(4-methoxyphenyl)-5-(3-hydroxy-4-aminophenyl-N,N,O-triacetate)dipyrromethane

Base Information

Chemical Name:trimethyl 1,1'-bis-(4-methoxyphenyl)-5-(3-hydroxy-4-aminophenyl-N,N,O-triacetate)dipyrromethane
CAS No.:864948-51-6
Molecular Formula:C₃₈H₃₉N₃O₉
Molecular Weight:681.742
Hs Code.:

Synonyms:trimethyl 1,1'-bis-(4-methoxyphenyl)-5-(3-hydroxy-4-aminophenyl-N,N,O-triacetate)dipyrromethane

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Chemical Property of trimethyl 1,1'-bis-(4-methoxyphenyl)-5-(3-hydroxy-4-aminophenyl-N,N,O-triacetate)dipyrromethane

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Technology Process of trimethyl 1,1'-bis-(4-methoxyphenyl)-5-(3-hydroxy-4-aminophenyl-N,N,O-triacetate)dipyrromethane

There total 3 articles about trimethyl 1,1'-bis-(4-methoxyphenyl)-5-(3-hydroxy-4-aminophenyl-N,N,O-triacetate)dipyrromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 4995-12-4
2-(4-methoxyphenyl)-1H-pyrrole

: 397883-29-3
2-formyl-2-methoxycarbonylmethoxy-N,N-bis(methoxycarbonylmethyl)aniline

: 864948-51-6
trimethyl 1,1'-bis-(4-methoxyphenyl)-5-(3-hydroxy-4-aminophenyl-N,N,O-triacetate)dipyrromethane

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 24h;
DOI:10.1039/b505969k

Reference yield:

: 450358-62-0
dimethyl 2,2'-((2-(2-methoxy-2-oxoethoxy)phenyl)azanediyl)diacetate

: 864948-51-6
trimethyl 1,1'-bis-(4-methoxyphenyl)-5-(3-hydroxy-4-aminophenyl-N,N,O-triacetate)dipyrromethane

Guidance literature:: Multi-step reaction with 2 steps

1: POCl₃

2: 42 percent / TFA / CH₂Cl₂ / 24 h

With trifluoroacetic acid; trichlorophosphate; In dichloromethane; 1: Vilsmeier formylation;
DOI:10.1039/b505969k

Reference yield:

: 198981-85-0
2-(4-methoxyphenyl)-1H-pyrrole-1-carboxylic acid 1,1-dimethylethyl ester

: 864948-51-6
trimethyl 1,1'-bis-(4-methoxyphenyl)-5-(3-hydroxy-4-aminophenyl-N,N,O-triacetate)dipyrromethane

Guidance literature:: Multi-step reaction with 2 steps

1: 180 mg / CH₃ONa / methanol / 24 h / Heating

2: 42 percent / TFA / CH₂Cl₂ / 24 h

With sodium methylate; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1039/b505969k