N-(2-(4-chlorophenyl)-3-methyl-5-oxo-5,6,7,8-tetrahydroquinolin-1(2H)-yl)benzamide

Base Information

Chemical Name:N-(2-(4-chlorophenyl)-3-methyl-5-oxo-5,6,7,8-tetrahydroquinolin-1(2H)-yl)benzamide
CAS No.:1564277-32-2
Molecular Formula:C₂₃H₂₁ClN₂O₂
Molecular Weight:392.885
Hs Code.:

Synonyms:N-(2-(4-chlorophenyl)-3-methyl-5-oxo-5,6,7,8-tetrahydroquinolin-1(2H)-yl)benzamide

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Chemical Property of N-(2-(4-chlorophenyl)-3-methyl-5-oxo-5,6,7,8-tetrahydroquinolin-1(2H)-yl)benzamide

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Technology Process of N-(2-(4-chlorophenyl)-3-methyl-5-oxo-5,6,7,8-tetrahydroquinolin-1(2H)-yl)benzamide

There total 3 articles about N-(2-(4-chlorophenyl)-3-methyl-5-oxo-5,6,7,8-tetrahydroquinolin-1(2H)-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 339241-95-1
C₁₃H₁₄N₂O₂

: 24654-54-4
3-(4-chlorophenyl)-2-methyl-2-propenal

: 1564277-32-2
N-(2-(4-chlorophenyl)-3-methyl-5-oxo-5,6,7,8-tetrahydroquinolin-1(2H)-yl)benzamide

Guidance literature:: With ethylenediamine diacetic acid; In N,N-dimethyl-formamide; at 115 ℃; for 0.133333h; Microwave irradiation;
DOI:10.3987/COM-13-12844

Reference yield:

: 613-94-5
benzoic acid hydrazide

: 1564277-32-2
N-(2-(4-chlorophenyl)-3-methyl-5-oxo-5,6,7,8-tetrahydroquinolin-1(2H)-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / water / 2 h / Reflux

2: ethylenediamine diacetic acid / N,N-dimethyl-formamide / 0.13 h / 115 °C / Microwave irradiation

With acetic acid; ethylenediamine diacetic acid; In water; N,N-dimethyl-formamide; 2: |Knoevenagel Condensation;
DOI:10.3987/COM-13-12844

Reference yield:

: 504-02-9
1,3-cylohexanedione

: 1564277-32-2
N-(2-(4-chlorophenyl)-3-methyl-5-oxo-5,6,7,8-tetrahydroquinolin-1(2H)-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / water / 2 h / Reflux

2: ethylenediamine diacetic acid / N,N-dimethyl-formamide / 0.13 h / 115 °C / Microwave irradiation

With acetic acid; ethylenediamine diacetic acid; In water; N,N-dimethyl-formamide; 2: |Knoevenagel Condensation;
DOI:10.3987/COM-13-12844