(S)-α-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-γ-butyrolactone

Base Information

Chemical Name:(S)-α-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-γ-butyrolactone
CAS No.:1190788-45-4
Molecular Formula:C₁₇H₂₂N₂O₆
Molecular Weight:350.371
Hs Code.:

Synonyms:(S)-α-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-γ-butyrolactone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-α-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-γ-butyrolactone

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Technology Process of (S)-α-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-γ-butyrolactone

There total 2 articles about (S)-α-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-γ-butyrolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: C₁₇H₂₃N₂O₇^(1-)*Na⁽¹⁺⁾

: 1190788-45-4
(S)-α-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-γ-butyrolactone

Guidance literature:: With tetrabutylammomium bromide; benzyl bromide; In acetone; for 24h; Reflux;
DOI:10.1016/j.tetasy.2009.07.003

Reference yield: 90.0%

: 1190788-44-3
(S)-α-[N(α)-(benzyloxycarbonyl)-N(β),N(β)-bis(tert-butyloxycarbonyl)hydrazino]-γ-butyrolactone

: 1190788-45-4
(S)-α-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-γ-butyrolactone

Guidance literature:: With magnesium(II) perchlorate; In acetonitrile; at 20 ℃;
DOI:10.1016/j.tetasy.2009.07.003

Reference yield: 100.0%

: 75-30-9
2-iodo-propane

: 1190788-45-4
(S)-α-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-γ-butyrolactone

: 1190788-50-1
isopropyl (2S)-2-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-4-hydroxybutanoate

Guidance literature:: (S)-α-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-γ-butyrolactone; With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 24h;

2-iodo-propane; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 30 ℃; for 76h;
DOI:10.1016/j.tetasy.2009.07.003