isopropyl (2S)-2-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-4-hydroxybutanoate

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Chemical Name:isopropyl (2S)-2-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-4-hydroxybutanoate
CAS No.:1190788-50-1
Molecular Formula:C₂₀H₃₀N₂O₇
Molecular Weight:410.467
Hs Code.:

Synonyms:isopropyl (2S)-2-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-4-hydroxybutanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of isopropyl (2S)-2-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-4-hydroxybutanoate

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Technology Process of isopropyl (2S)-2-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-4-hydroxybutanoate

There total 2 articles about isopropyl (2S)-2-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-4-hydroxybutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 75-30-9
2-iodo-propane

: 1190788-45-4
(S)-α-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-γ-butyrolactone

: 1190788-50-1
isopropyl (2S)-2-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-4-hydroxybutanoate

Guidance literature:: (S)-α-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-γ-butyrolactone; With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 24h;

2-iodo-propane; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 30 ℃; for 76h;
DOI:10.1016/j.tetasy.2009.07.003

Reference yield: 49.0%

: 1190788-45-4
(S)-α-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-γ-butyrolactone

: 75-26-3
isopropyl bromide

: 1190788-50-1
isopropyl (2S)-2-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-4-hydroxybutanoate

Guidance literature:: (S)-α-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-γ-butyrolactone; With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 24h;

isopropyl bromide; With tetrabutylammomium bromide; In acetone; at 30 ℃; for 76h;
DOI:10.1016/j.tetasy.2009.07.003

Reference yield: 61.0%

: 1190788-50-1
isopropyl (2S)-2-[N(α)-(benzyloxycarbonyl)-N(β)-(tert-butyloxycarbonyl)hydrazino]-4-hydroxybutanoate

: 1190788-51-2
C₂₀H₂₈N₂O₆

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.07.003