1,11-bis-[phenoxy-(3,5-dicarbaldehyde)]-3,6,9-trioxo undecane

Base Information

Chemical Name:1,11-bis-[phenoxy-(3,5-dicarbaldehyde)]-3,6,9-trioxo undecane
CAS No.:1370287-52-7
Molecular Formula:C₂₄H₂₆O₉
Molecular Weight:458.465
Hs Code.:

Synonyms:1,11-bis-[phenoxy-(3,5-dicarbaldehyde)]-3,6,9-trioxo undecane

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Chemical Property of 1,11-bis-[phenoxy-(3,5-dicarbaldehyde)]-3,6,9-trioxo undecane

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Technology Process of 1,11-bis-[phenoxy-(3,5-dicarbaldehyde)]-3,6,9-trioxo undecane

There total 4 articles about 1,11-bis-[phenoxy-(3,5-dicarbaldehyde)]-3,6,9-trioxo undecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 371919-11-8
1,11-bis-[phenoxy-(3,5-dihydroxymethyl)]-3,6,9-trioxo-undecane

: 1370287-52-7
1,11-bis-[phenoxy-(3,5-dicarbaldehyde)]-3,6,9-trioxo undecane

Guidance literature:: With silica gel; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jm200860b

Reference yield:

: 1370287-47-0
1,11-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6,9-trioxo-undecane

: 1370287-52-7
1,11-bis-[phenoxy-(3,5-dicarbaldehyde)]-3,6,9-trioxo undecane

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

2: silica gel; pyridinium chlorochromate / tetrahydrofuran; dichloromethane / 1 h / 20 °C

With lithium aluminium tetrahydride; silica gel; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm200860b

Reference yield:

: 37860-51-8
tetraethylene glycol di(p-toluenesulfonate)

: 1370287-52-7
1,11-bis-[phenoxy-(3,5-dicarbaldehyde)]-3,6,9-trioxo undecane

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 10 h / Inert atmosphere; Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

3: silica gel; pyridinium chlorochromate / tetrahydrofuran; dichloromethane / 1 h / 20 °C

With lithium aluminium tetrahydride; silica gel; potassium carbonate; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jm200860b