1,11-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6,9-trioxo-undecane

Base Information

Chemical Name:1,11-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6,9-trioxo-undecane
CAS No.:1370287-47-0
Molecular Formula:C₂₈H₃₄O₁₃
Molecular Weight:578.57
Hs Code.:

Synonyms:1,11-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6,9-trioxo-undecane

Suppliers and Price of 1,11-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6,9-trioxo-undecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1,11-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6,9-trioxo-undecane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1,11-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6,9-trioxo-undecane

There total 2 articles about 1,11-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6,9-trioxo-undecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 37860-51-8
tetraethylene glycol di(p-toluenesulfonate)

: 13036-02-7
Dimethyl 5-hydroxyisophthalate

: 1370287-47-0
1,11-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6,9-trioxo-undecane

Guidance literature:: With potassium carbonate; In acetonitrile; for 10h; Inert atmosphere; Reflux;
DOI:10.1021/jm200860b

Reference yield:

: 112-60-7
Tetraethylene glycol

: 1370287-47-0
1,11-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6,9-trioxo-undecane

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / tetrahydrofuran / 0.5 h / Cooling with ice

1.2: 3 h / 20 °C / Cooling with ice

2.1: potassium carbonate / acetonitrile / 10 h / Inert atmosphere; Reflux

With potassium carbonate; sodium hydroxide; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jm200860b