2-(acetoxymethyl)-4-methoxy-5-<(2-methoxypyrid-5-yl)methyl>-1-acetoxybenzene

Base Information

Chemical Name:2-(acetoxymethyl)-4-methoxy-5-<(2-methoxypyrid-5-yl)methyl>-1-acetoxybenzene
CAS No.:117653-29-9
Molecular Formula:C₁₉H₂₁NO₆
Molecular Weight:359.379
Hs Code.:

Synonyms:2-(acetoxymethyl)-4-methoxy-5-<(2-methoxypyrid-5-yl)methyl>-1-acetoxybenzene

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Chemical Property of 2-(acetoxymethyl)-4-methoxy-5-<(2-methoxypyrid-5-yl)methyl>-1-acetoxybenzene

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Technology Process of 2-(acetoxymethyl)-4-methoxy-5-<(2-methoxypyrid-5-yl)methyl>-1-acetoxybenzene

There total 3 articles about 2-(acetoxymethyl)-4-methoxy-5-<(2-methoxypyrid-5-yl)methyl>-1-acetoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105189-48-8
4-methoxy-3-<(6-methoxypyridin-3-yl)methyl>phenol

: 117653-29-9
2-(acetoxymethyl)-4-methoxy-5-<(2-methoxypyrid-5-yl)methyl>-1-acetoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 1) boric acid, 2) 30percent H₂SO₄ / 1) ethylene glycol, 130 deg C, 0.5 h, 2) 80 deg C to room temperature

2: 75 percent / NaBH₄ / methanol; dioxane / 0.5 h / Ambient temperature

3: pyridine / 1 h / 100 °C

With pyridine; sodium tetrahydroborate; sulfuric acid; boric acid; In 1,4-dioxane; methanol;
DOI:10.1021/jm00122a009

Reference yield:

: 117653-28-8
2-formyl-4-methoxy-5-<(2-methoxypyrid-5-yl)methyl>phenol

: 117653-29-9
2-(acetoxymethyl)-4-methoxy-5-<(2-methoxypyrid-5-yl)methyl>-1-acetoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / NaBH₄ / methanol; dioxane / 0.5 h / Ambient temperature

2: pyridine / 1 h / 100 °C

With pyridine; sodium tetrahydroborate; In 1,4-dioxane; methanol;
DOI:10.1021/jm00122a009