dimethyl 2-(3-(4-chlorophenyl)prop-2-ynyl)-2-(3-methylbut-2-enyl)malonate

Base Information

Chemical Name:dimethyl 2-(3-(4-chlorophenyl)prop-2-ynyl)-2-(3-methylbut-2-enyl)malonate
CAS No.:1542558-89-3
Molecular Formula:C₁₉H₂₁ClO₄
Molecular Weight:348.826
Hs Code.:

Synonyms:dimethyl 2-(3-(4-chlorophenyl)prop-2-ynyl)-2-(3-methylbut-2-enyl)malonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl 2-(3-(4-chlorophenyl)prop-2-ynyl)-2-(3-methylbut-2-enyl)malonate

Chemical Property:

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Technology Process of dimethyl 2-(3-(4-chlorophenyl)prop-2-ynyl)-2-(3-methylbut-2-enyl)malonate

There total 1 articles about dimethyl 2-(3-(4-chlorophenyl)prop-2-ynyl)-2-(3-methylbut-2-enyl)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-39-8
bromochlorobenzene

: 107473-14-3
dimethyl 2-propargyl-2-prenylmalonate

: 1542558-89-3
dimethyl 2-(3-(4-chlorophenyl)prop-2-ynyl)-2-(3-methylbut-2-enyl)malonate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; isopropylamine; at 20 ℃;
DOI:10.1039/c3cc48339h

Reference yield: 74.0%

: 1542558-89-3
dimethyl 2-(3-(4-chlorophenyl)prop-2-ynyl)-2-(3-methylbut-2-enyl)malonate

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: dimethyl 4′-chloro-6-(prop-1-en-2-yl)-2-tosyl-5,6-dihydro-[1,1′-biphenyl]-4,4(3H)-dicarboxylate

Guidance literature:: With tert.-butylhydroperoxide; iodine; In water; at 80 ℃; for 24h; Inert atmosphere; Green chemistry;
DOI:10.1021/acs.joc.5b02161

Reference yield: 54.0%

: 1542558-89-3
dimethyl 2-(3-(4-chlorophenyl)prop-2-ynyl)-2-(3-methylbut-2-enyl)malonate

: 100-52-7
benzaldehyde

: 1542560-25-7
dimethyl 4-benzoyl-7-chloro-9,9-dimethyl-9,9a-dihydro-1H-fluorene-2,2(3H)-dicarboxylate

Guidance literature:: With tert.-butylhydroperoxide; Trimethylacetic acid; In acetonitrile; at 120 ℃; for 48h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c3cc48339h