9-benzenesulfonyloxy-10-methoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinolinyl-7-ium chloride

Base Information

Chemical Name:9-benzenesulfonyloxy-10-methoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinolinyl-7-ium chloride
CAS No.:16312-34-8
Molecular Formula:C₂₅H₂₀NO₆S*Cl
Molecular Weight:497.956
Hs Code.:

Synonyms:9-benzenesulfonyloxy-10-methoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinolinyl-7-ium chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-benzenesulfonyloxy-10-methoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinolinyl-7-ium chloride

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Technology Process of 9-benzenesulfonyloxy-10-methoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinolinyl-7-ium chloride

There total 2 articles about 9-benzenesulfonyloxy-10-methoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinolinyl-7-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15401-69-1
berberrubine chloride

: 98-09-9
benzenesulfonyl chloride

: 16312-34-8
9-benzenesulfonyloxy-10-methoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinolinyl-7-ium chloride

Guidance literature:: With pyridine; In chloroform; for 2h; Heating / reflux;

Reference yield:

: 633-65-8
berberine chloride

: 16312-34-8
9-benzenesulfonyloxy-10-methoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinolinyl-7-ium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 0.5 h / 190 °C

2: pyridine / chloroform / 2 h / Reflux

With pyridine; In chloroform;

Reference yield:

: 16312-34-8
9-benzenesulfonyloxy-10-methoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinolinyl-7-ium chloride

: 875288-94-1
9-benzenesulfonyloxy-10-methoxy-5,8,13,13a-tetrahydro-6H-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinoline

Guidance literature:: 9-benzenesulfonyloxy-10-methoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinolinyl-7-ium chloride; With sodium tetrahydroborate; In methanol; for 1h; Heating / reflux;

With water; In methanol;