9-benzenesulfonyloxy-10-methoxy-5,8,13,13a-tetrahydro-6H-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinoline

Base Information

Chemical Name:9-benzenesulfonyloxy-10-methoxy-5,8,13,13a-tetrahydro-6H-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinoline
CAS No.:875288-94-1
Molecular Formula:C₂₅H₂₃NO₆S
Molecular Weight:465.527
Hs Code.:

Synonyms:9-benzenesulfonyloxy-10-methoxy-5,8,13,13a-tetrahydro-6H-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-benzenesulfonyloxy-10-methoxy-5,8,13,13a-tetrahydro-6H-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinoline

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Technology Process of 9-benzenesulfonyloxy-10-methoxy-5,8,13,13a-tetrahydro-6H-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinoline

There total 4 articles about 9-benzenesulfonyloxy-10-methoxy-5,8,13,13a-tetrahydro-6H-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16312-34-8
9-benzenesulfonyloxy-10-methoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinolinyl-7-ium chloride

: 875288-94-1
9-benzenesulfonyloxy-10-methoxy-5,8,13,13a-tetrahydro-6H-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinoline

Guidance literature:: 9-benzenesulfonyloxy-10-methoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinolinyl-7-ium chloride; With sodium tetrahydroborate; In methanol; for 1h; Heating / reflux;

With water; In methanol;

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 17388-17-9
(+/-)-nandinine

: 875288-94-1
9-benzenesulfonyloxy-10-methoxy-5,8,13,13a-tetrahydro-6H-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinoline

Guidance literature:: With triethylamine; In dichloromethane; Reflux;
DOI:10.1016/j.bioorg.2022.105665

Reference yield:

: 15401-69-1
berberrubine chloride

: 875288-94-1
9-benzenesulfonyloxy-10-methoxy-5,8,13,13a-tetrahydro-6H-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / chloroform / 2 h / Reflux

2: sodium tetrahydroborate; methanol / 1 h / Reflux

With pyridine; methanol; sodium tetrahydroborate; In chloroform;