copper(III) 5,15-bis(pentafluorophenyl)-10-(3-azidomethylphenyl)corrole

Base Information

• Chemical Name: copper(III) 5,15-bis(pentafluorophenyl)-10-(3-azidomethylphenyl)corrole
• CAS No.: 1620027-97-5
• Molecular Formula: C₃₈H₁₄CuF₁₀N₇
• Molecular Weight: 822.106

Synonyms:copper(III) 5,15-bis(pentafluorophenyl)-10-(3-azidomethylphenyl)corrole

Chemical Property of copper(III) 5,15-bis(pentafluorophenyl)-10-(3-azidomethylphenyl)corrole

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Technology Process of copper(III) 5,15-bis(pentafluorophenyl)-10-(3-azidomethylphenyl)corrole

There total 3 articles about copper(III) 5,15-bis(pentafluorophenyl)-10-(3-azidomethylphenyl)corrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(bromomethyl)benzaldehyde (82072-23-9) → copper(III) 5,15-bis(pentafluorophenyl)-10-(3-azidomethylphenyl)corrole (1620027-97-5)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride / methanol; water / 1 h / 20 °C

2: sodium azide; N-benzyl-N,N,N-triethylammonium chloride / N,N-dimethyl-formamide / 20 °C

3: dichloromethane; methanol / 0.5 h / 20 °C

With hydrogenchloride; sodium azide; N-benzyl-N,N,N-triethylammonium chloride; In methanol; dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1021/ic500714h

Reference yield:

5,15-bis-(pentafluorophenyl)-10-(3-bromomethylphenyl)corrole (1620027-94-2) → copper(III) 5,15-bis(pentafluorophenyl)-10-(3-azidomethylphenyl)corrole (1620027-97-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium azide; N-benzyl-N,N,N-triethylammonium chloride / N,N-dimethyl-formamide / 20 °C

2: dichloromethane; methanol / 0.5 h / 20 °C

With sodium azide; N-benzyl-N,N,N-triethylammonium chloride; In methanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ic500714h

Reference yield:

5-(pentafluorophenyl)dipyrromethane (167482-91-9) → copper(III) 5,15-bis(pentafluorophenyl)-10-(3-azidomethylphenyl)corrole (1620027-97-5)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride / methanol; water / 1 h / 20 °C

2: sodium azide; N-benzyl-N,N,N-triethylammonium chloride / N,N-dimethyl-formamide / 20 °C

3: dichloromethane; methanol / 0.5 h / 20 °C

With hydrogenchloride; sodium azide; N-benzyl-N,N,N-triethylammonium chloride; In methanol; dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1021/ic500714h

upstream raw materials:

5-(pentafluorophenyl)dipyrromethane

3-(bromomethyl)benzaldehyde

5,15-bis-(pentafluorophenyl)-10-(3-bromomethylphenyl)corrole

Downstream raw materials:

1-[(10-(3-methylenephenyl))-5,15-bis(pentafluorophenyl)copper-(III)corrole]-4-[(10-(4-oxymethylene))-5,15-bis(pentafluorophenyl)-iron(III)corrole(bis(acetonitrile))]triazole

copper(III) 5,15-bis(pentafluorophenyl)-10-(3-methynyl-(4-methanol-1,2,3-triazol-1-yl)phenyl)corrole

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