copper(III) 5,15-bis(pentafluorophenyl)-10-(3-methynyl-(4-methanol-1,2,3-triazol-1-yl)phenyl)corrole

Base Information

Chemical Name:copper(III) 5,15-bis(pentafluorophenyl)-10-(3-methynyl-(4-methanol-1,2,3-triazol-1-yl)phenyl)corrole
CAS No.:1620028-03-6
Molecular Formula:C₄₁H₁₈CuF₁₀N₇O
Molecular Weight:878.17
Hs Code.:

Synonyms:copper(III) 5,15-bis(pentafluorophenyl)-10-(3-methynyl-(4-methanol-1,2,3-triazol-1-yl)phenyl)corrole

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Chemical Property of copper(III) 5,15-bis(pentafluorophenyl)-10-(3-methynyl-(4-methanol-1,2,3-triazol-1-yl)phenyl)corrole

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Technology Process of copper(III) 5,15-bis(pentafluorophenyl)-10-(3-methynyl-(4-methanol-1,2,3-triazol-1-yl)phenyl)corrole

There total 4 articles about copper(III) 5,15-bis(pentafluorophenyl)-10-(3-methynyl-(4-methanol-1,2,3-triazol-1-yl)phenyl)corrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1620027-97-5
copper(III) 5,15-bis(pentafluorophenyl)-10-(3-azidomethylphenyl)corrole

: 107-19-7
propargyl alcohol

: 1620028-03-6
copper(III) 5,15-bis(pentafluorophenyl)-10-(3-methynyl-(4-methanol-1,2,3-triazol-1-yl)phenyl)corrole

Guidance literature:: With copper (I) acetate; In dichloromethane; at 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/ic500714h

Reference yield:

: 82072-23-9
3-(bromomethyl)benzaldehyde

: 1620028-03-6
copper(III) 5,15-bis(pentafluorophenyl)-10-(3-methynyl-(4-methanol-1,2,3-triazol-1-yl)phenyl)corrole

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / methanol; water / 1 h / 20 °C

2: sodium azide; N-benzyl-N,N,N-triethylammonium chloride / N,N-dimethyl-formamide / 20 °C

3: dichloromethane; methanol / 0.5 h / 20 °C

4: copper (I) acetate / dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

With hydrogenchloride; sodium azide; N-benzyl-N,N,N-triethylammonium chloride; copper (I) acetate; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ic500714h

Reference yield:

: 1620027-94-2
5,15-bis-(pentafluorophenyl)-10-(3-bromomethylphenyl)corrole

: 1620028-03-6
copper(III) 5,15-bis(pentafluorophenyl)-10-(3-methynyl-(4-methanol-1,2,3-triazol-1-yl)phenyl)corrole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide; N-benzyl-N,N,N-triethylammonium chloride / N,N-dimethyl-formamide / 20 °C

2: dichloromethane; methanol / 0.5 h / 20 °C

3: copper (I) acetate / dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

With sodium azide; N-benzyl-N,N,N-triethylammonium chloride; copper (I) acetate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ic500714h