cis-iso-propyl-4,4'-(1R,2S₉-3-(isopropoxycarbonyl)cyclopent-3-ene-1,2-diyl)dibenzoate

Base Information

• Chemical Name: cis-iso-propyl-4,4'-(1R,2S₉-3-(isopropoxycarbonyl)cyclopent-3-ene-1,2-diyl)dibenzoate
• CAS No.: 1265848-33-6
• Molecular Formula: C₂₉H₃₄O₆
• Molecular Weight: 478.585

Synonyms:cis-iso-propyl-4,4'-(1R,2S₉-3-(isopropoxycarbonyl)cyclopent-3-ene-1,2-diyl)dibenzoate

Chemical Property of cis-iso-propyl-4,4'-(1R,2S₉-3-(isopropoxycarbonyl)cyclopent-3-ene-1,2-diyl)dibenzoate

Chemical Property:

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Technology Process of cis-iso-propyl-4,4'-(1R,2S₉-3-(isopropoxycarbonyl)cyclopent-3-ene-1,2-diyl)dibenzoate

There total 1 articles about cis-iso-propyl-4,4'-(1R,2S₉-3-(isopropoxycarbonyl)cyclopent-3-ene-1,2-diyl)dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

titanium(IV) isopropylate (546-68-9) + 4-((E)-3-oxoprop-1-enyl)-benzoic acid methyl ester (73166-52-6,78024-60-9) → cis-iso-propyl-4,4'-((1S,2R)-3-(isopropoxycarbonyl)cyclopent-3-ene-1,2-diyl)dibenzoate + cis-iso-propyl-4,4'-(1R,2S9-3-(isopropoxycarbonyl)cyclopent-3-ene-1,2-diyl)dibenzoate (1265848-33-6)

Guidance literature:

With BF₄^(1-)*C₃₁H₂₈N₃O₃S⁽¹⁺⁾; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; In toluene; at 23 ℃; for 36h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;

DOI:10.1021/ol103112v

upstream raw materials:

titanium(IV) isopropylate

4-((E)-3-oxoprop-1-enyl)-benzoic acid methyl ester

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