1-benzyl-2,5,6-trichlorobenzimidazole

Base Information

Chemical Name:1-benzyl-2,5,6-trichlorobenzimidazole
CAS No.:142372-26-7
Molecular Formula:C₁₄H₉Cl₃N₂
Molecular Weight:311.598
Hs Code.:

Synonyms:1-benzyl-2,5,6-trichlorobenzimidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzyl-2,5,6-trichlorobenzimidazole

Chemical Property:

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Technology Process of 1-benzyl-2,5,6-trichlorobenzimidazole

There total 4 articles about 1-benzyl-2,5,6-trichlorobenzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 100-39-0
benzyl bromide

: 16865-11-5
2,5,6-trichloro-1H-benzo[d]imidazole

: 142372-26-7
1-benzyl-2,5,6-trichlorobenzimidazole

Guidance literature:: With sodium hydroxide; In acetonitrile; Heating;
DOI:10.1021/jm970559i

Reference yield:

: 7732-18-5
water

: 100-39-0
benzyl bromide

: 584-08-7
potassium carbonate

: 16865-11-5
2,5,6-trichloro-1H-benzo[d]imidazole

: 142372-26-7
1-benzyl-2,5,6-trichlorobenzimidazole

Guidance literature:: In methanol; chloroform; acetonitrile;

Reference yield:

: 5348-42-5
4,5-Dichloro-1,2-phenylenediamine

: 142372-26-7
1-benzyl-2,5,6-trichlorobenzimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 0.5 h / 150 °C

2: POCl₃, HCl / 3 h / 150 °C

3: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF, 1 h

With hydrogenchloride; sodium hydride; trichlorophosphate;
DOI:10.1021/jm960442e