methyl 2-(4-((2,4-diaminopyrimidin-5-yl)methyl)-2,6-dimethoxyphenoxy)acetate

Base Information

Chemical Name:methyl 2-(4-((2,4-diaminopyrimidin-5-yl)methyl)-2,6-dimethoxyphenoxy)acetate
CAS No.:83166-78-3
Molecular Formula:C₁₆H₂₀N₄O₅
Molecular Weight:348.359
Hs Code.:

Synonyms:methyl 2-(4-((2,4-diaminopyrimidin-5-yl)methyl)-2,6-dimethoxyphenoxy)acetate

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Chemical Property of methyl 2-(4-((2,4-diaminopyrimidin-5-yl)methyl)-2,6-dimethoxyphenoxy)acetate

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Technology Process of methyl 2-(4-((2,4-diaminopyrimidin-5-yl)methyl)-2,6-dimethoxyphenoxy)acetate

There total 1 articles about methyl 2-(4-((2,4-diaminopyrimidin-5-yl)methyl)-2,6-dimethoxyphenoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 96-32-2
bromoacetic acid methyl ester

: 21253-58-7
2,4-diamino-5-(3,5-dimethoxy-4-hydroxybenzyl)pyrimidine

: 83166-78-3
methyl 2-(4-((2,4-diaminopyrimidin-5-yl)methyl)-2,6-dimethoxyphenoxy)acetate

Guidance literature:: 2,4-diamino-5-(3,5-dimethoxy-4-hydroxybenzyl)pyrimidine; With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; Inert atmosphere;

bromoacetic acid methyl ester; at 20 ℃; Inert atmosphere;
DOI:10.1021/ja500170h

Reference yield: 70.0%

: 83166-78-3
methyl 2-(4-((2,4-diaminopyrimidin-5-yl)methyl)-2,6-dimethoxyphenoxy)acetate

: 78025-77-1
2-(4-((2,4-diaminopyrimidin-5-yl)methyl)-2,6-dimethoxyphenoxy)acetic acid

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃; for 1h;
DOI:10.1021/ja500170h

Reference yield:

: 83166-78-3
methyl 2-(4-((2,4-diaminopyrimidin-5-yl)methyl)-2,6-dimethoxyphenoxy)acetate

: 1578196-69-6
C₃₀H₄₈N₆O₉

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / methanol / 1 h / 20 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 h / 5 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja500170h