6-Benzyl-2-chloro-7,7-dioxo-6,7-dihydro-4H-1,7λ⁶-dithia-4,6-diaza-inden-5-one

Base Information

• Chemical Name: 6-Benzyl-2-chloro-7,7-dioxo-6,7-dihydro-4H-1,7λ⁶-dithia-4,6-diaza-inden-5-one
• CAS No.: 214916-55-9
• Molecular Formula: C₁₂H₉ClN₂O₃S₂
• Molecular Weight: 328.8

Synonyms:6-Benzyl-2-chloro-7,7-dioxo-6,7-dihydro-4H-1,7λ⁶-dithia-4,6-diaza-inden-5-one

Chemical Property of 6-Benzyl-2-chloro-7,7-dioxo-6,7-dihydro-4H-1,7λ⁶-dithia-4,6-diaza-inden-5-one

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Technology Process of 6-Benzyl-2-chloro-7,7-dioxo-6,7-dihydro-4H-1,7λ⁶-dithia-4,6-diaza-inden-5-one

There total 1 articles about 6-Benzyl-2-chloro-7,7-dioxo-6,7-dihydro-4H-1,7λ⁶-dithia-4,6-diaza-inden-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

2-(N-benzylsulfamoyl)-5-chlorothiophene-3-carboxylic acid → 2-Benzyl-5-chloro-1,1-dioxo-1,2-dihydro-1λ6-thieno[3,2-d]isothiazol-3-one + 6-Benzyl-2-chloro-7,7-dioxo-6,7-dihydro-4H-1,7λ6-dithia-4,6-diaza-inden-5-one (214916-55-9)

Guidance literature:

With diphenylphosphoranyl azide; triethylamine; In toluene; at 80 ℃; for 24h;

DOI:10.1021/jm9802012

Reference yield:

chloroacetonitrile (107-14-2) + 6-Benzyl-2-chloro-7,7-dioxo-6,7-dihydro-4H-1,7λ6-dithia-4,6-diaza-inden-5-one (214916-55-9) → (6-Benzyl-2-chloro-5,7,7-trioxo-6,7-dihydro-5H-1,7λ6-dithia-4,6-diaza-inden-4-yl)-acetonitrile (214916-53-7)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 10 deg C, 15 min, 2.) DMF, from 50 to 60 deg C, 40 h;

DOI:10.1021/jm9802012

Reference yield:

benzyl bromide (100-39-0) + 6-Benzyl-2-chloro-7,7-dioxo-6,7-dihydro-4H-1,7λ6-dithia-4,6-diaza-inden-5-one (214916-55-9) → 4,6-Dibenzyl-2-chloro-7,7-dioxo-6,7-dihydro-4H-1,7λ6-dithia-4,6-diaza-inden-5-one

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 10 deg C, 15 min, 2.) DMF, from 50 to 60 deg C, 40 h;

DOI:10.1021/jm9802012

Downstream raw materials:

(6-Benzyl-2-chloro-5,7,7-trioxo-6,7-dihydro-5H-1,7λ⁶-dithia-4,6-diaza-inden-4-yl)-acetonitrile

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