2-(3-N,N-diethylaminocarbonylphenyl)-3-(2-methoxyphenyl)-4-thiazolidinone

Base Information

Chemical Name:2-(3-N,N-diethylaminocarbonylphenyl)-3-(2-methoxyphenyl)-4-thiazolidinone
CAS No.:1395435-52-5
Molecular Formula:C₂₁H₂₄N₂O₃S
Molecular Weight:384.499
Hs Code.:

Synonyms:2-(3-N,N-diethylaminocarbonylphenyl)-3-(2-methoxyphenyl)-4-thiazolidinone

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Chemical Property of 2-(3-N,N-diethylaminocarbonylphenyl)-3-(2-methoxyphenyl)-4-thiazolidinone

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Technology Process of 2-(3-N,N-diethylaminocarbonylphenyl)-3-(2-methoxyphenyl)-4-thiazolidinone

There total 6 articles about 2-(3-N,N-diethylaminocarbonylphenyl)-3-(2-methoxyphenyl)-4-thiazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1395435-10-5
3-(3-(2-methoxyphenyl)-4-oxo-2-thiazolidinyl)benzoic acid

: 109-89-7
diethylamine

: 1395435-52-5
2-(3-N,N-diethylaminocarbonylphenyl)-3-(2-methoxyphenyl)-4-thiazolidinone

Guidance literature:: 3-(3-(2-methoxyphenyl)-4-oxo-2-thiazolidinyl)benzoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-d₆-formamide; for 0.0833333h; Cooling with ice; Inert atmosphere;

diethylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 3.25h; Inert atmosphere;
DOI:10.1016/j.ejmech.2014.04.068

Reference yield:

: 90-04-0
2-methoxy-phenylamine

: 1395435-52-5
2-(3-N,N-diethylaminocarbonylphenyl)-3-(2-methoxyphenyl)-4-thiazolidinone

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 140 °C / Inert atmosphere

2.1: lithium hydroxide monohydrate; water / methanol / 20 °C / Cooling with ice; Inert atmosphere

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-d₆-formamide / 0.08 h / Cooling with ice; Inert atmosphere

3.2: 3.25 h / 0 - 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; toluene; N,N-dimethyl-d₆-formamide;
DOI:10.1016/j.ejmech.2014.04.068

Reference yield:

: 52178-50-4
Methyl 3-formylbenzoate

: 1395435-52-5
2-(3-N,N-diethylaminocarbonylphenyl)-3-(2-methoxyphenyl)-4-thiazolidinone

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 140 °C / Inert atmosphere

2.1: lithium hydroxide monohydrate; water / methanol / 20 °C / Cooling with ice; Inert atmosphere

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-d₆-formamide / 0.08 h / Cooling with ice; Inert atmosphere

3.2: 3.25 h / 0 - 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; toluene; N,N-dimethyl-d₆-formamide;
DOI:10.1016/j.ejmech.2014.04.068