FeBd2(Cl2Gm)(BF)2

Base Information

Chemical Name:FeBd2(Cl2Gm)(BF)2
CAS No.:380456-14-4
Molecular Formula:C₃₀H₂₀B₂Cl₂F₂FeN₆O₆
Molecular Weight:746.897
Hs Code.:

Synonyms:FeBd2(Cl2Gm)(BF)2

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Chemical Property of FeBd2(Cl2Gm)(BF)2

Chemical Property:

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Technology Process of FeBd2(Cl2Gm)(BF)2

There total 3 articles about FeBd2(Cl2Gm)(BF)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 199733-44-3
[Fe(α-benzyldioximato)2(BF2)2(acetonitrile)2]

: 2038-44-0
dichloroglyoxime

: 380456-14-4
FeBd2(Cl2Gm)(BF)2

Guidance literature:: With triethylamine; BF₃*OEt₂; In nitromethane; Fe-contg. compd. and an excess of dichloroglyoxime were dissolved/suspended in dry nitromethane-hexamethyldisiloxane mixt. with stirring under Ar; NEt3, BF3OEt2 and chloroform were added dropwise; heating to b.p.; BF3*OEt2 addn.; the solvent was distd. off with stirring; the mixt. was allowed to cool to room temp.; the solid was filtered off, washed with methanol, Et2O, and then with hexane, and dried in vac.; elem. anal.;
DOI:10.1039/b107021p

Reference yield:

: 23873-81-6
benzildioxime

: 380456-14-4
FeBd2(Cl2Gm)(BF)2

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol

2: diethyl ether

3: boron trifluoride diethyl etherate; triethylamine / nitromethane

With boron trifluoride diethyl etherate; triethylamine; In diethyl ether; nitromethane; ethanol;
DOI:10.1080/10426507.2012.744012

Reference yield:

: iron(II)bis(α-benzoyldioximate)(py)2

: 380456-14-4
FeBd2(Cl2Gm)(BF)2

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: boron trifluoride diethyl etherate; triethylamine / nitromethane

With boron trifluoride diethyl etherate; triethylamine; In diethyl ether; nitromethane;
DOI:10.1080/10426507.2012.744012