(2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:(2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-α-D-mannopyranoside
CAS No.:1361016-59-2
Molecular Formula:C₂₄H₃₀O₅S
Molecular Weight:430.565
Hs Code.:

Synonyms:(2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Suppliers and Price of (2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-α-D-mannopyranoside

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Technology Process of (2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-α-D-mannopyranoside

There total 4 articles about (2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1361016-58-1
(2-methyl-5-tert-butylphenyl) 1-thio-α-D-mannopyranoside

: 100-52-7
benzaldehyde

: 1361016-59-2
(2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Guidance literature:: With (1S)-10-camphorsulfonic acid; In dichloromethane; at 20 ℃; for 5h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.bmc.2011.12.048

Reference yield: 45.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 1361016-58-1
(2-methyl-5-tert-butylphenyl) 1-thio-α-D-mannopyranoside

: 1361016-59-2
(2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Guidance literature:: With iron(III) chloride; In toluene; acetonitrile; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/ejoc.201600457

Reference yield:

: 3458-28-4
D-Mannose

: 1361016-59-2
(2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; acetic anhydride / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: (1S)-10-camphorsulfonic acid / dichloromethane / 5 h / 20 °C / Molecular sieve; Inert atmosphere

With pyridine; (1S)-10-camphorsulfonic acid; acetic anhydride; In dichloromethane;
DOI:10.1016/j.bmc.2011.12.048