N^α-acetyl-p--L-phenylalanylglycine methylamide

Base Information

Chemical Name:N^α-acetyl-p--L-phenylalanylglycine methylamide
CAS No.:95484-31-4
Molecular Formula:C₂₁H₃₁N₅O₅
Molecular Weight:433.508
Hs Code.:

N<sup>α</sup>-acetyl-p-<N'-(5-oxohexyl)ureido>-L-phenylalanylglycine methylamide

Synonyms:N^α-acetyl-p--L-phenylalanylglycine methylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N^α-acetyl-p--L-phenylalanylglycine methylamide

Chemical Property:

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Technology Process of N^α-acetyl-p--L-phenylalanylglycine methylamide

There total 3 articles about N^α-acetyl-p--L-phenylalanylglycine methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 95513-71-6
N^α-acetyl-p--L-phenylalanylglycine benzyl ester

: 74-89-5
methylamine

: 95484-31-4
N^α-acetyl-p--L-phenylalanylglycine methylamide

Guidance literature:: In methanol; for 15h; Ambient temperature;
DOI:10.1021/jm50001a017

Reference yield:

: 3128-07-2
6-oxoheptanoic acid

: 95484-31-4
N^α-acetyl-p--L-phenylalanylglycine methylamide

Guidance literature:: Multi-step reaction with 3 steps

1: diphenylphosphoryl azide (DPPA), triethylamine / benzene / 1.) 23 deg C, 30 min, 2.) reflux, 15 min

2: benzene / 0.25 h / Ambient temperature

3: 63 percent / methanol / 15 h / Ambient temperature

With diphenylphosphoranyl azide; triethylamine; In methanol; benzene;
DOI:10.1021/jm50001a017

Reference yield:

: 70486-31-6
6-Isocyanato-hexan-2-one

: 95484-31-4
N^α-acetyl-p--L-phenylalanylglycine methylamide

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 0.25 h / Ambient temperature

2: 63 percent / methanol / 15 h / Ambient temperature

In methanol; benzene;
DOI:10.1021/jm50001a017