6β,9α-dihydroxy-8,13-epoxy-7β-[3-(4-morpholinomethyl)benzoyloxy]-1α-tert-butyldimethylsilyloxy-labd-14-en-11-one

Base Information

Chemical Name:6β,9α-dihydroxy-8,13-epoxy-7β-[3-(4-morpholinomethyl)benzoyloxy]-1α-tert-butyldimethylsilyloxy-labd-14-en-11-one
CAS No.:913976-18-8
Molecular Formula:C₃₈H₅₉NO₈Si
Molecular Weight:685.974
Hs Code.:

Synonyms:6β,9α-dihydroxy-8,13-epoxy-7β-[3-(4-morpholinomethyl)benzoyloxy]-1α-tert-butyldimethylsilyloxy-labd-14-en-11-one

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Chemical Property of 6β,9α-dihydroxy-8,13-epoxy-7β-[3-(4-morpholinomethyl)benzoyloxy]-1α-tert-butyldimethylsilyloxy-labd-14-en-11-one

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Technology Process of 6β,9α-dihydroxy-8,13-epoxy-7β-[3-(4-morpholinomethyl)benzoyloxy]-1α-tert-butyldimethylsilyloxy-labd-14-en-11-one

There total 1 articles about 6β,9α-dihydroxy-8,13-epoxy-7β-[3-(4-morpholinomethyl)benzoyloxy]-1α-tert-butyldimethylsilyloxy-labd-14-en-11-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 67451-81-4
3-((morpholin-4-yl)methyl)benzoic acid

: 105535-46-4
1α-<(tert-butyldimethylsilyl)oxy>-8,13-epoxy-6β,7β,9α-trihydroxylabd-14-en-11-one

: 913976-18-8
6β,9α-dihydroxy-8,13-epoxy-7β-[3-(4-morpholinomethyl)benzoyloxy]-1α-tert-butyldimethylsilyloxy-labd-14-en-11-one

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; for 16h;

Reference yield: 55.0%

: 913976-18-8
6β,9α-dihydroxy-8,13-epoxy-7β-[3-(4-morpholinomethyl)benzoyloxy]-1α-tert-butyldimethylsilyloxy-labd-14-en-11-one

: 913976-19-9
7β,9α-dihydroxy-8,13-epoxy-6β-[3-(4-morpholinomethyl)benzoyloxy]-1α-tert-butyldimethylsilyloxy-labd-14-en-11-one

Guidance literature:: With sodium hydroxide; In diethyl ether; water; acetonitrile; at 20 ℃; for 16h;

Reference yield:

: 913976-18-8
6β,9α-dihydroxy-8,13-epoxy-7β-[3-(4-morpholinomethyl)benzoyloxy]-1α-tert-butyldimethylsilyloxy-labd-14-en-11-one

: 913976-20-2
7β-acetoxy-8,13-epoxy-9α-hydroxy-6β-[3-(4-morpholinomethyl)benzoyloxy]-1α-tert-butyldimethylsilyloxy-labd-14-en-11-one

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / NaOH / acetonitrile; diethyl ether; H₂O / 16 h / 20 °C

2: 98 percent / DCC; DMAP / ethyl acetate

With dmap; sodium hydroxide; dicyclohexyl-carbodiimide; In diethyl ether; water; ethyl acetate; acetonitrile;