n-Hexyl acetyl-N-cyclohexylmalonamate

Base Information

• Chemical Name: n-Hexyl acetyl-N-cyclohexylmalonamate
• CAS No.: 73453-44-8
• Molecular Formula: C₁₇H₂₉NO₄
• Molecular Weight: 311.422

Synonyms:n-Hexyl acetyl-N-cyclohexylmalonamate

Chemical Property of n-Hexyl acetyl-N-cyclohexylmalonamate

Chemical Property:

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Technology Process of n-Hexyl acetyl-N-cyclohexylmalonamate

There total 5 articles about n-Hexyl acetyl-N-cyclohexylmalonamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

Ethyl Acetyl-N-cyclohexylmalonamate (73453-43-7) → N-cyclohexylacetamide (1124-53-4) + N,N'-dicyclohexyl-malonamide (10256-00-5) + n-Hexyl acetyl-N-cyclohexylmalonamate (73453-44-8) + Acetyl-N,N'-dicyclohexylmalonamide (73453-46-0)

Guidance literature:

With hexan-1-ol; for 0.333333h; Further byproducts given; Heating;

DOI:10.1021/jo01300a036

Reference yield:

Ethyl Acetyl-N-cyclohexylmalonamate (73453-43-7) + hexan-1-ol (111-27-3) → N-cyclohexylacetamide (1124-53-4) + N,N'-dicyclohexyl-malonamide (10256-00-5) + n-Hexyl acetyl-N-cyclohexylmalonamate (73453-44-8) + Acetyl-N,N'-dicyclohexylmalonamide (73453-46-0)

Guidance literature:

for 0.333333h; Further byproducts given; Heating;

DOI:10.1021/jo01300a036

Reference yield:

Ethyl Acetyl-N-cyclohexylmalonamate (73453-43-7) → N-cyclohexylacetamide (1124-53-4) + N,N'-dicyclohexyl-malonamide (10256-00-5) + Di-n-hexyl acetylmalonate (73453-45-9) + n-Hexyl N-cyclohexylmalonamide (73453-47-1) + n-Hexyl acetyl-N-cyclohexylmalonamate (73453-44-8) + Acetyl-N,N'-dicyclohexylmalonamide (73453-46-0)

Guidance literature:

With hexan-1-ol; for 0.333333h; Heating;

DOI:10.1021/jo01300a036

upstream raw materials:

Ethyl Acetyl-N-cyclohexylmalonamate

hexan-1-ol

ethyl acetoacetate

Cyclohexyl isocyanate

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