Boronic acid, B-[2-(difluoroMethyl)-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-

Base Information

• Chemical Name: Boronic acid, B-[2-(difluoroMethyl)-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-
• CAS No.: 1014613-45-6
• Molecular Formula: C₁₄H₁₁BF₂N₂O₄S
• Molecular Weight: 352.126
• Mol file: 1014613-45-6.mol

Synonyms:[2-(difluoromethyl)-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]boronic acid

Chemical Property of Boronic acid, B-[2-(difluoroMethyl)-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

B-[2-(difluoromethyl)-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-Boronicacid 97.00% ^*data from reagent suppliers

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Technology Process of Boronic acid, B-[2-(difluoroMethyl)-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-

There total 1 articles about Boronic acid, B-[2-(difluoroMethyl)-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C20H23BF2N2O4S → [2-(difluoromethyl)-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]boronic acid (1014613-45-6)

Guidance literature:

With hydrogenchloride; water; In tetrahydrofuran; hexanes; at -78 ℃; for 0.0833333h;

Reference yield:

[2-(difluoromethyl)-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]boronic acid (1014613-45-6) + 1-[(5-bromo-2-thienyl)sulfonyl]-1H-imidazole (1089669-75-9) → 2-(difluoromethyl)-4-[5-(1H-imidazol-1-ylsulfonyl)-2-thienyl]-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridine (1089669-63-5)

Guidance literature:

With sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; water; at 120 ℃; for 0.5h; Microwave irradiation;

Reference yield:

[2-(difluoromethyl)-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]boronic acid (1014613-45-6) + 6-chloro-N-(1,1-dioxidotetrahydro-2H-thiopyran-4-yl)-3-pyridinesulfonamide (1089669-43-1) → 6-[2-(difluoromethyl)-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-N-(1,1-dioxidotetrahydro-2H-thiopyran-4-yl)-3-pyridinesulfonamide (1089669-52-2)

Guidance literature:

With sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; water; at 150 ℃; for 1h; Microwave irradiation;

Downstream raw materials:

2-(difluoromethyl)-4-[5-(1H-imidazol-1-ylsulfonyl)-2-thienyl]-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridine

6-[2-(difluoromethyl)-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-N-(1,1-dioxidotetrahydro-2H-thiopyran-4-yl)-3-pyridinesulfonamide

C₂₄H₂₂F₂N₄O₆S₃

1,1-dimethylethyl 4-[({6-[2-(difluoromethyl)-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-3-pyridinyl}sulfonyl)amino]-1-piperidinecarboxylate

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