Technology Process of 1-(4-chlorophenyl)-1H-indazol-3-amine
There total 5 articles about 1-(4-chlorophenyl)-1H-indazol-3-amine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper immobilized at polyimide covalent organic framework;
In
methanol; water;
at 20 ℃;
for 10h;
DOI:10.1039/c8gc02611d
- Guidance literature:
-
With
copper(l) iodide; (R,R)-N,N'-dimethyl-1,2-diaminocyclohexane; potassium carbonate;
In
1,4-dioxane;
at 110 ℃;
for 18h;
DOI:10.1002/ejoc.202101245
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydroxylamine / ethanol; water / 75 °C / Inert atmosphere
2.1: sodium methylate / ethanol; methanol / 0.17 h / 20 °C / Inert atmosphere
2.2: 3 h / Reflux; Inert atmosphere
3.1: potassium carbonate; copper diacetate / N,N-dimethyl acetamide / 1 h / 110 °C / Microwave irradiation
With
hydroxylamine; sodium methylate; copper diacetate; potassium carbonate;
In
methanol; ethanol; N,N-dimethyl acetamide; water;
DOI:10.1021/acs.joc.1c03057
