3-(3-chloro-4-hydroxy-5-methylsulfanylbenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

Base Information

Chemical Name:3-(3-chloro-4-hydroxy-5-methylsulfanylbenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole
CAS No.:1285572-89-5
Molecular Formula:C₁₅H₁₂ClNO₄S₂
Molecular Weight:369.85
Hs Code.:

Synonyms:3-(3-chloro-4-hydroxy-5-methylsulfanylbenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

Suppliers and Price of 3-(3-chloro-4-hydroxy-5-methylsulfanylbenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-(3-chloro-4-hydroxy-5-methylsulfanylbenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-(3-chloro-4-hydroxy-5-methylsulfanylbenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

There total 11 articles about 3-(3-chloro-4-hydroxy-5-methylsulfanylbenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 624-92-0
Dimethyldisulphide

: 1285575-12-3
3-(3-chloro-4-hydroxy-5-iodobenzoyl)-1,1-dioxo-2,3-dihydro-1,3-benzothiazole

: 1285572-89-5
3-(3-chloro-4-hydroxy-5-methylsulfanylbenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

Guidance literature:: With zinc; [2,2]bipyridinyl; nickel dibromide; In N,N-dimethyl-formamide; at 80 ℃; for 1.5h;

Reference yield:

: 1285575-14-5
3-(3-chloro-4-methoxy-5-methylsulfanylbenzoyl)-1,1-dioxo-2,3-dihydro-1,3-benzothiazole

: 1285572-89-5
3-(3-chloro-4-hydroxy-5-methylsulfanylbenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

Guidance literature:: 3-(3-chloro-4-methoxy-5-methylsulfanylbenzoyl)-1,1-dioxo-2,3-dihydro-1,3-benzothiazole; With lithium chloride; In N,N-dimethyl-formamide; at 120 ℃; for 20h;

With hydrogenchloride; In water; N,N-dimethyl-formamide;

Reference yield:

: 3964-57-6
methyl 4-hydroxy-3-chlorobenzoate

: 1285572-89-5
3-(3-chloro-4-hydroxy-5-methylsulfanylbenzoyl)-1,1-dioxo-1,2-dihydro-3H-1,3-benzothiazole

Guidance literature:: Multi-step reaction with 8 steps

1: N-iodo-succinimide; trifluorormethanesulfonic acid / methanol; dichloromethane / 2 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C

3: lithium hydroxide monohydrate; water / tetrahydrofuran / 19 h / 20 °C

4: thionyl chloride / N,N-dimethyl-formamide / toluene / 15 h / 60 °C

5: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

6: 3-chloro-benzenecarboperoxoic acid / tetrahydrofuran / 1.5 h / 20 °C

7: lithium chloride / N,N-dimethyl-formamide / 2.5 h / 120 °C

8: zinc / [2,2]bipyridinyl; nickel dibromide / N,N-dimethyl-formamide / 1.5 h / 80 °C

With N-iodo-succinimide; thionyl chloride; lithium hydroxide monohydrate; trifluorormethanesulfonic acid; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium chloride; zinc; [2,2]bipyridinyl; N,N-dimethyl-formamide; nickel dibromide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;