3,5-dibenzyl-2-oxo-3,5-diazatricyclo<5.3.1.0^4,9>decane

Base Information

Chemical Name:3,5-dibenzyl-2-oxo-3,5-diazatricyclo<5.3.1.0^4,9>decane
CAS No.:107384-01-0
Molecular Formula:C₂₃H₂₆N₂O
Molecular Weight:346.472
Hs Code.:

3,5-dibenzyl-2-oxo-3,5-diazatricyclo<5.3.1.0<sup>4,9</sup>>decane

Synonyms:3,5-dibenzyl-2-oxo-3,5-diazatricyclo<5.3.1.0^4,9>decane

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Chemical Property of 3,5-dibenzyl-2-oxo-3,5-diazatricyclo<5.3.1.0^4,9>decane

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Technology Process of 3,5-dibenzyl-2-oxo-3,5-diazatricyclo<5.3.1.0^4,9>decane

There total 9 articles about 3,5-dibenzyl-2-oxo-3,5-diazatricyclo<5.3.1.0^4,9>decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 554-95-0
benzene-1,3,5-tricarboxylic acid

: 107384-01-0
3,5-dibenzyl-2-oxo-3,5-diazatricyclo<5.3.1.0^4,9>decane

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / HCl )g) / 1 h / Heating

2: 98 percent / acetic acid, hydrogen / platinum oxide / 3.5 h / 25 °C / 1034.3 - 2585.7 Torr

3: 83.7 percent / lithium aluminum hydride / tetrahydrofuran / 16 h / Heating

4: 70 percent / dimethyl sulfoxide, oxalyl chloride / CH₂Cl₂ / 2.25 h / -55 °C

5: Drierite, Bio-Rad resin AG 50W-X₈ / toluene / 4.5 h / Heating

With hydrogenchloride; calcium sulfate; lithium aluminium tetrahydride; oxalyl dichloride; Bio-Rad resin AG 50W-X₈; hydrogen; acetic acid; dimethyl sulfoxide; platinum(IV) oxide; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jo00385a002

Reference yield:

: 4105-92-4
triethyl benzene-1,3,5-tricarboxylate

: 107384-01-0
3,5-dibenzyl-2-oxo-3,5-diazatricyclo<5.3.1.0^4,9>decane

Guidance literature:: Multi-step reaction with 4 steps

1: 99.5 percent / H₂, acetic acid / platinum oxide / 3.5 h / 25 °C / 1034.3 - 2585.7 Torr

2: 81 percent / lithium aluminum hydride / diethyl ether / 16 h / Heating

3: 70 percent / dimethyl sulfoxide, oxalyl chloride / CH₂Cl₂ / 2.25 h / -55 °C

4: Drierite, Bio-Rad resin AG 50W-X₈ / toluene / 4.5 h / Heating

With calcium sulfate; lithium aluminium tetrahydride; oxalyl dichloride; Bio-Rad resin AG 50W-X₈; hydrogen; acetic acid; dimethyl sulfoxide; platinum(IV) oxide; In diethyl ether; dichloromethane; toluene;
DOI:10.1021/jo00385a002

Reference yield:

: 2672-58-4
1,3,5-tris-(methoxycarbonyl)benzene

: 107384-01-0
3,5-dibenzyl-2-oxo-3,5-diazatricyclo<5.3.1.0^4,9>decane

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / H₂, acetic acid / platinum oxide / 3.5 h / 25 °C / 1034.3 - 2585.7 Torr

2: 57 percent / lithium aluminum hydride / diethyl ether / 16 h / Heating

3: 70 percent / dimethyl sulfoxide, oxalyl chloride / CH₂Cl₂ / 2.25 h / -55 °C

4: Drierite, Bio-Rad resin AG 50W-X₈ / toluene / 4.5 h / Heating

With calcium sulfate; lithium aluminium tetrahydride; oxalyl dichloride; Bio-Rad resin AG 50W-X₈; hydrogen; acetic acid; dimethyl sulfoxide; platinum(IV) oxide; In diethyl ether; dichloromethane; toluene;
DOI:10.1021/jo00385a002