2,3-O-diacetyl-5-O-tert-butyldiphenylsilyl-D-ribofuranosyl acetate

Base Information Edit

Chemical Name:2,3-O-diacetyl-5-O-tert-butyldiphenylsilyl-D-ribofuranosyl acetate
CAS No.:688809-73-6
Molecular Formula:C₂₇H₃₄O₈Si
Molecular Weight:514.648
Hs Code.:
Mol file:688809-73-6.mol

Synonyms:2,3-O-diacetyl-5-O-tert-butyldiphenylsilyl-D-ribofuranosyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-O-diacetyl-5-O-tert-butyldiphenylsilyl-D-ribofuranosyl acetate Edit

Chemical Property:

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Technology Process of 2,3-O-diacetyl-5-O-tert-butyldiphenylsilyl-D-ribofuranosyl acetate

There total 2 articles about 2,3-O-diacetyl-5-O-tert-butyldiphenylsilyl-D-ribofuranosyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 532-20-7,613-83-2,7261-25-8,7687-39-0,13221-22-2,14795-83-6,15761-67-8,20074-49-1,25545-03-3,25545-04-4,32445-75-3,34436-17-4,36441-93-7,36468-53-8,37110-85-3,37388-49-1,38029-69-5,40461-77-6,40461-89-0,41546-19-4,41546-20-7,41546-21-8,41546-26-3,41546-29-6,41546-30-9,41546-31-0,126872-16-0,131064-98-7
D-Ribose

: 108-24-7
acetic anhydride

: 688809-73-6
2,3-O-diacetyl-5-O-tert-butyldiphenylsilyl-D-ribofuranosyl acetate

Guidance literature:: D-Ribose; tert-butylchlorodiphenylsilane; With 1H-imidazole; In DMF (N,N-dimethyl-formamide); at 0 - 20 ℃;

With potassium hydrogensulfate; In DMF (N,N-dimethyl-formamide); water; at 20 ℃; for 0.5h;

acetic anhydride; With pyridine; potassium hydrogensulfate; more than 3 stages;

Reference yield:

: 532-20-7,613-83-2,7261-25-8,7687-39-0,13221-22-2,14795-83-6,15761-67-8,20074-49-1,25545-03-3,25545-04-4,32445-75-3,34436-17-4,36441-93-7,36468-53-8,37110-85-3,37388-49-1,38029-69-5,40461-77-6,40461-89-0,41546-19-4,41546-20-7,41546-21-8,41546-26-3,41546-29-6,41546-30-9,41546-31-0,126872-16-0,131064-98-7
D-Ribose

: 108-24-7
acetic anhydride

: 58479-61-1
tert-butylchlorodiphenylsilane

: 688809-73-6
2,3-O-diacetyl-5-O-tert-butyldiphenylsilyl-D-ribofuranosyl acetate

: C₂₇H₃₄O₈Si

Guidance literature:: D-Ribose; tert-butylchlorodiphenylsilane; With pyridine; Cooling with ice; Inert atmosphere;

acetic anhydride; for 18h; Overall yield = 43.3 percent; Overall yield = 6.81 g; Cooling with ice; Inert atmosphere;