(1S,2R)-2-((S)-1-Hydroxy-allyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

Base Information

Chemical Name:(1S,2R)-2-((S)-1-Hydroxy-allyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide
CAS No.:184292-96-4
Molecular Formula:C₁₇H₂₃NO₂
Molecular Weight:273.375
Hs Code.:

Synonyms:(1S,2R)-2-((S)-1-Hydroxy-allyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R)-2-((S)-1-Hydroxy-allyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

Chemical Property:

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Technology Process of (1S,2R)-2-((S)-1-Hydroxy-allyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

There total 1 articles about (1S,2R)-2-((S)-1-Hydroxy-allyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1826-67-1
vinyl magnesium bromide

: 172016-00-1
(1S,2R)-2-Formyl-1-phenyl-cyclopropanecarboxylic acid diethylamide

: 184292-96-4
(1S,2R)-2-((S)-1-Hydroxy-allyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

Guidance literature:: In tetrahydrofuran; at -20 ℃; for 2h;
DOI:10.1021/jm960495w

Reference yield:

: 184292-96-4
(1S,2R)-2-((S)-1-Hydroxy-allyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

: [1-((1R,2S)-2-Diethylcarbamoyl-2-phenyl-cyclopropyl)-allyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) (CF₃CO)2O / 1.) MeCN, RT, 1 h, 2.) MeCN, EtOH, reflux, 16 h

2: 99 percent / iPrNH₂, N-chlorosuccinimide / methanol / 2 h / Ambient temperature

With N-chloro-succinimide; isopropylamine; trifluoroacetic anhydride; In methanol;
DOI:10.1021/jm960495w

Reference yield:

: 23974-72-3
sodium phenylselenide

: 184292-96-4
(1S,2R)-2-((S)-1-Hydroxy-allyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

: (1S,2S)-1-Phenyl-2-((E)-3-phenylselanyl-propenyl)-cyclopropanecarboxylic acid diethylamide

Guidance literature:: With trifluoroacetic anhydride; Yield given. Multistep reaction; 1.) MeCN, RT, 1 h, 2.) MeCN, EtOH, reflux, 16 h;
DOI:10.1021/jm960495w