Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(C₆H₅)2)Br⁽¹⁺⁾*Br^(1-)=[Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(C₆H₅)2)Br]Br

Base Information

• Chemical Name: Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(C₆H₅)2)Br⁽¹⁺⁾*Br^(1-)=[Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(C₆H₅)2)Br]Br
• CAS No.: 220528-51-8
• Molecular Formula: Br*C₃₄H₃₃BrP₃Pd
• Molecular Weight: 800.785

Synonyms:Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(C₆H₅)2)Br⁽¹⁺⁾*Br^(1-)=[Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(C₆H₅)2)Br]Br

Chemical Property of Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(C₆H₅)2)Br⁽¹⁺⁾*Br^(1-)=[Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(C₆H₅)2)Br]Br

Chemical Property:

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Technology Process of Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(C₆H₅)2)Br⁽¹⁺⁾*Br^(1-)=[Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(C₆H₅)2)Br]Br

There total 3 articles about Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(C₆H₅)2)Br⁽¹⁺⁾*Br^(1-)=[Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(C₆H₅)2)Br]Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

sodium bromide (7647-15-6) + palladium dichloride + bis(2-diphenylphosphinoethyl)phenylphosphine (23582-02-7) → Pd((C6H5)2P(CH2)2P(C6H5)(CH2)2P(C6H5)2)Br(1+)*Br(1-)=[Pd((C6H5)2P(CH2)2P(C6H5)(CH2)2P(C6H5)2)Br]Br (220528-51-8)

Guidance literature:

In dichloromethane; water; stirring (24 h); evapn. (vac.), recrystn. (CH2Cl2/n-hexane, 2/1); elem. anal.;

DOI:10.1016/S0277-5387(98)00307-6

Reference yield: 80.0%

[chloro(bis[(2-diphenylphosphino)ethyl]phenylphosphine)palladium(II)] chloride (85744-68-9) + sodium bromide (7647-15-6) → Pd((C6H5)2P(CH2)2P(C6H5)(CH2)2P(C6H5)2)Br(1+)*Br(1-)=[Pd((C6H5)2P(CH2)2P(C6H5)(CH2)2P(C6H5)2)Br]Br (220528-51-8)

Guidance literature:

NaBr was added to Pd-complex; elem. anal.;

DOI:10.1016/S0020-1693(00)00329-7

Reference yield:

bis(2-diphenylphosphinoethyl)phenylphosphine (23582-02-7) → Pd((C6H5)2P(CH2)2P(C6H5)(CH2)2P(C6H5)2)Br(1+)*Br(1-)=[Pd((C6H5)2P(CH2)2P(C6H5)(CH2)2P(C6H5)2)Br]Br (220528-51-8)

Guidance literature:

Multi-step reaction with 2 steps

1: water; dichloromethane

In dichloromethane; water;

DOI:10.1016/S0020-1693(00)00329-7

upstream raw materials:

sodium bromide

bis(2-diphenylphosphinoethyl)phenylphosphine

[chloro(bis[(2-diphenylphosphino)ethyl]phenylphosphine)palladium(II)] chloride

Downstream raw materials:

Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(O)(C₆H₅)2)2⁽²⁺⁾*PdBr₄^(2-)=[Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(O)(C₆H₅)2)2][PdBr₄]

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