[Ru(NH₃)(2,6-bis(3-triphenylsilyl-2-sulfanylphenylthiomethyl)pyridine^(2-))]

Base Information

• Chemical Name: [Ru(NH₃)(2,6-bis(3-triphenylsilyl-2-sulfanylphenylthiomethyl)pyridine^(2-))]
• CAS No.: 894768-33-3
• Molecular Formula: C₅₅H₄₆N₂RuS₄Si₂
• Molecular Weight: 1020.49

Synonyms:[Ru(NH₃)(2,6-bis(3-triphenylsilyl-2-sulfanylphenylthiomethyl)pyridine^(2-))]

Chemical Property of [Ru(NH₃)(2,6-bis(3-triphenylsilyl-2-sulfanylphenylthiomethyl)pyridine^(2-))]

Chemical Property:

Purity/Quality:

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Technology Process of [Ru(NH₃)(2,6-bis(3-triphenylsilyl-2-sulfanylphenylthiomethyl)pyridine^(2-))]

There total 2 articles about [Ru(NH₃)(2,6-bis(3-triphenylsilyl-2-sulfanylphenylthiomethyl)pyridine^(2-))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

Ru(NO)(2,6-bis(3-triphenylsilyl-2-sulfanylphenylthiomethyl)pyridine(2-))Br * tetrahydrofuran + hydrazine (302-01-2,78206-91-4,119775-10-9,75013-58-0) → [Ru(NH3)(2,6-bis(3-triphenylsilyl-2-sulfanylphenylthiomethyl)pyridine(2-))] (894768-33-3) + dinitrogen monoxide (10024-97-2)

Guidance literature:

In tetrahydrofuran; methanol; byproducts: HBr; (N2); N2H4 in THF added to a soln. of Ru complex in MeOH, stirred for 0-25 min at room temp.; filtered, washed (MeOH, Et2O), dried (vac.); elem. anal.;

DOI:10.1021/ic060096j

Reference yield:

Ru(NO)(2,6-bis(3-triphenylsilyl-2-sulfanylphenylthiomethyl)pyridine(2-))Br * tetrahydrofuran → [Ru(NH3)(2,6-bis(3-triphenylsilyl-2-sulfanylphenylthiomethyl)pyridine(2-))] (894768-33-3)

Guidance literature:

In further solvent(s); Electrochem. Process; (N2); at -1.05 V vs SCE in CH2Cl2/N(C4H9)4PF6;

DOI:10.1021/ic060096j

Reference yield:

[Ru(NH3)(2,6-bis(3-triphenylsilyl-2-sulfanylphenylthiomethyl)pyridine(2-))] (894768-33-3) → [(NH3)Ru(μ-2,6-bis(3-triphenylsilyl-2-sulfanylphenylthiomethyl)pyridine(2-))Ru(2,6-bis(3-triphenylsilyl-2-sulfanylphenylthiomethyl)pyridine(2-))]

Guidance literature:

In dichloromethane; byproducts: NH3; (N2); at 20°C for 2 d;

DOI:10.1021/ic060096j

upstream raw materials:

hydrazine

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