C₆₀H₆₆N₂O₆

Base Information

• Chemical Name: C₆₀H₆₆N₂O₆
• CAS No.: 952684-26-3
• Molecular Formula: C₆₀H₆₆N₂O₆
• Molecular Weight: 911.194
• Mol file: 952684-26-3.mol

Synonyms:C₆₀H₆₆N₂O₆

Chemical Property of C₆₀H₆₆N₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₀H₆₆N₂O₆

There total 5 articles about C₆₀H₆₆N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N,N'-di(2-ethylhexyl)-1,7-dibromoperylene-3,4,9,10-bisdicarboximide (851786-15-7) + para-tert-butylphenol (98-54-4) → C60H66N2O6 (952684-26-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 1h;

DOI:10.1016/j.tetlet.2011.12.080

Reference yield:

2-Ethylhexylamine (104-75-6) + para-tert-butylphenol (98-54-4) + perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride (128-69-8) → C60H66N2O6 (952684-26-3) + C60H66N2O6

Guidance literature:

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride; With sulfuric acid; bromine; iodine; at 85 ℃; for 24h;

2-Ethylhexylamine; In propionic acid; for 48h; Reflux;

para-tert-butylphenol; With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 7h; Overall yield = 80 %; Inert atmosphere;

DOI:10.1016/j.tet.2015.07.032

Reference yield:

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride (128-69-8) → C60H66N2O6 (952684-26-3)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine / 48 h / 120 °C

2: bromine / dichloromethane / 24 h / 50 °C

3: potassium carbonate / N,N-dimethyl-formamide / 1 h / 80 °C

With pyridine; bromine; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.tetlet.2011.12.080

upstream raw materials:

N,N'-di(2-ethylhexyl)-1,7-dibromoperylene-3,4,9,10-bisdicarboximide

para-tert-butylphenol

2-Ethylhexylamine

2,9-bis(2-ethylhexyl)anthra[2,1,9-def:6,5,10-d',e',f']diisoquinoline-1,3,8,10(2H,9H)-tetraone