2-hydroxy-1-deuteroformylbenzene

Base Information

• Chemical Name: 2-hydroxy-1-deuteroformylbenzene
• CAS No.: 71367-06-1
• Molecular Formula: C₇H₆O₂
• Molecular Weight: 123.115
• Mol file: 71367-06-1.mol

Synonyms:2-hydroxy-1-deuteroformylbenzene

Chemical Property of 2-hydroxy-1-deuteroformylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2-hydroxy-1-deuteroformylbenzene

There total 18 articles about 2-hydroxy-1-deuteroformylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2-α-deuterio-(tetrahydropyran-2-yloxy)benzaldehyde → 2-hydroxy-1-deuteroformylbenzene (71367-06-1)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; at 20 ℃; for 10h;

DOI:10.1002/chem.200305629

Reference yield: 90.0%

2-deutero-2-(2'-hydroxyphenyl)-1,3-dithiane (1330147-04-0) → 2-hydroxy-1-deuteroformylbenzene (71367-06-1)

Guidance literature:

With methanol; mercury(II) trifluoroacetate; In chloroform; Inert atmosphere;

DOI:10.1021/ol200256a

Reference yield: 47.0%

salicylaldehyde (90-02-8) → 2-hydroxy-1-deuteroformylbenzene (71367-06-1)

Guidance literature:

With 1,3-bis[2,6-bis(1-methylethyl)phenyl]-4,5-dihydro-1H-imidazolium bromide; water-d2; sodium hydrogencarbonate; In toluene; at 80 ℃; for 12h;

upstream raw materials:

<α,D2>-o-hydroxybenzyl alcohol

(2-methoxymethoxy-phenyl)-trimethylsilanyloxy-acetonitrile

2-(methoxymethoxy)benzaldehyde

2-(tetrahydropyran-2-yloxy)phenyl bromide

Downstream raw materials:

C₁₀H₁₁⁽²⁾HO₂

C₁₅H₁₄⁽²⁾HNO

4-(2-deuteroformylphenoxy)but-2-enoic acid ethyl ester

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