Technology Process of 3,5-diisopropoxybenzylchloride
There total 2 articles about 3,5-diisopropoxybenzylchloride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine; dichlorotriphenylphosphorane;
In
acetonitrile;
at 0 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1016/j.tetlet.2020.151856
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 48 h / 50 °C / Inert atmosphere
2: lithium aluminium tetrahydride / tetrahydrofuran / 21 - 23 °C / Inert atmosphere
3: dichlorotriphenylphosphorane; N-ethyl-N,N-diisopropylamine / acetonitrile / 0.5 h / 0 °C / Inert atmosphere
With
lithium aluminium tetrahydride; tetra-(n-butyl)ammonium iodide; potassium carbonate; N-ethyl-N,N-diisopropylamine; dichlorotriphenylphosphorane;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tetlet.2020.151856
- Guidance literature:
-
With
copper(l) iodide; tetra-(n-butyl)ammonium iodide; potassium carbonate;
In
acetonitrile;
at 40 ℃;
Inert atmosphere;
DOI:10.1016/j.tetlet.2020.151856
