3,5-diisopropoxybenzylchloride

Base Information

Chemical Name:3,5-diisopropoxybenzylchloride
CAS No.:1228424-86-9
Molecular Formula:C₁₃H₁₉ClO₂
Molecular Weight:242.746
Hs Code.:

Synonyms:3,5-diisopropoxybenzylchloride

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Chemical Property of 3,5-diisopropoxybenzylchloride

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Technology Process of 3,5-diisopropoxybenzylchloride

There total 2 articles about 3,5-diisopropoxybenzylchloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 94169-63-8
(3,5-diisopropoxyphenyl)methanol

: 1228424-86-9
3,5-diisopropoxybenzylchloride

Guidance literature:: With N-ethyl-N,N-diisopropylamine; dichlorotriphenylphosphorane; In acetonitrile; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tetlet.2020.151856

Reference yield:

: 99-10-5
3,5-Dihydroxybenzoic acid

: 1228424-86-9
3,5-diisopropoxybenzylchloride

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 48 h / 50 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 21 - 23 °C / Inert atmosphere

3: dichlorotriphenylphosphorane; N-ethyl-N,N-diisopropylamine / acetonitrile / 0.5 h / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; tetra-(n-butyl)ammonium iodide; potassium carbonate; N-ethyl-N,N-diisopropylamine; dichlorotriphenylphosphorane; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tetlet.2020.151856

Reference yield: 76.0%

: 1228424-86-9
3,5-diisopropoxybenzylchloride

: 623-47-2
propynoic acid ethyl ester

: C₁₈H₂₄O₄

Guidance literature:: With copper(l) iodide; tetra-(n-butyl)ammonium iodide; potassium carbonate; In acetonitrile; at 40 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2020.151856