2-methoxy-4-hydrazinylbenzoic acid hydrochloride

Base Information

Chemical Name:2-methoxy-4-hydrazinylbenzoic acid hydrochloride
CAS No.:1338815-21-6
Molecular Formula:C₈H₁₀N₂O₃*ClH
Molecular Weight:218.64
Hs Code.:

Synonyms:2-methoxy-4-hydrazinylbenzoic acid hydrochloride

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Chemical Property of 2-methoxy-4-hydrazinylbenzoic acid hydrochloride

Chemical Property:

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Technology Process of 2-methoxy-4-hydrazinylbenzoic acid hydrochloride

There total 1 articles about 2-methoxy-4-hydrazinylbenzoic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2486-80-8
4-amino-2-methoxybenzoic acid

: 1338815-21-6
2-methoxy-4-hydrazinylbenzoic acid hydrochloride

Guidance literature:: 4-amino-2-methoxybenzoic acid; With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 5.08333h;

With hydrogenchloride; tin(ll) chloride; In water; at 0 - 20 ℃; for 64h;

Reference yield:

: 59997-51-2
trimethylacetylacetonitrile

: 1338815-21-6
2-methoxy-4-hydrazinylbenzoic acid hydrochloride

: 1338815-22-7
4-(5-amino-3-tert-butyl-1H-pyrazol-1-yl)-2-methoxybenzoic acid

Guidance literature:: trimethylacetylacetonitrile; 2-methoxy-4-hydrazinylbenzoic acid hydrochloride; With hydrogenchloride; In ethanol; water; for 28h; Reflux;

With sodium hydroxide; In ethanol; water; at 20 ℃; for 20h;

Reference yield:

: 1338815-21-6
2-methoxy-4-hydrazinylbenzoic acid hydrochloride

: 1338815-23-8
3-tert-butyl-1-(3-methoxy-4-((triisopropylsilyloxy)methyl)phenyl)-1H-pyrazol-5-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / ethanol; water / 28 h / Reflux

1.2: 20 h / 20 °C

2.1: diborane / tetrahydrofuran / 46.08 h / 0 - 20 °C / Inert atmosphere

2.2: 0.17 h / 20 °C

3.1: 1H-imidazole / tetrahydrofuran / 139 h / 20 °C / Inert atmosphere

With 1H-imidazole; hydrogenchloride; diborane; In tetrahydrofuran; ethanol; water;