6-benzyloxy-4-bromo-3-(4-methoxy-phenyl)-1-(2-nitro-benzenesulfonyl)-2,3-dihydro-1H-indole

Base Information

Chemical Name:6-benzyloxy-4-bromo-3-(4-methoxy-phenyl)-1-(2-nitro-benzenesulfonyl)-2,3-dihydro-1H-indole
CAS No.:1269631-60-8
Molecular Formula:C₂₈H₂₃BrN₂O₆S
Molecular Weight:595.47
Hs Code.:

Synonyms:6-benzyloxy-4-bromo-3-(4-methoxy-phenyl)-1-(2-nitro-benzenesulfonyl)-2,3-dihydro-1H-indole

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Chemical Property of 6-benzyloxy-4-bromo-3-(4-methoxy-phenyl)-1-(2-nitro-benzenesulfonyl)-2,3-dihydro-1H-indole

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Technology Process of 6-benzyloxy-4-bromo-3-(4-methoxy-phenyl)-1-(2-nitro-benzenesulfonyl)-2,3-dihydro-1H-indole

There total 5 articles about 6-benzyloxy-4-bromo-3-(4-methoxy-phenyl)-1-(2-nitro-benzenesulfonyl)-2,3-dihydro-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1269631-66-4
N-[2-(4-benzyloxy-2,6-dibromo-phenyl)-2-(4-methoxy-phenyl)-ethyl]-2-nitro-benzenesulfonamide

: 1269631-60-8
6-benzyloxy-4-bromo-3-(4-methoxy-phenyl)-1-(2-nitro-benzenesulfonyl)-2,3-dihydro-1H-indole

Guidance literature:: With copper(l) iodide; cesium acetate; In dimethyl sulfoxide; at 20 ℃; for 21h;
DOI:10.1002/asia.201000544

Reference yield:

: 1269631-59-5
5-benzyloxy-1,3-dibromo-2-[1-(4-methoxy-phenyl)-2-nitro-ethyl]-benzene

: 1269631-60-8
6-benzyloxy-4-bromo-3-(4-methoxy-phenyl)-1-(2-nitro-benzenesulfonyl)-2,3-dihydro-1H-indole

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; iron; iron(II) chloride / ethanol / 8 h / Reflux

2: sodium hydrogencarbonate / dichloromethane; water / 15 h / 20 °C

3: copper(l) iodide; cesium acetate / dimethyl sulfoxide / 21 h / 20 °C

With hydrogenchloride; copper(l) iodide; cesium acetate; iron; sodium hydrogencarbonate; iron(II) chloride; In ethanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1002/asia.201000544

Reference yield:

: C₂₂H₂₁Br₂NO₂

: 1269631-60-8
6-benzyloxy-4-bromo-3-(4-methoxy-phenyl)-1-(2-nitro-benzenesulfonyl)-2,3-dihydro-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / dichloromethane; water / 15 h / 20 °C

2: copper(l) iodide; cesium acetate / dimethyl sulfoxide / 21 h / 20 °C

With copper(l) iodide; cesium acetate; sodium hydrogencarbonate; In dichloromethane; water; dimethyl sulfoxide;
DOI:10.1002/asia.201000544