(1R,2R,3S,4R,5R)-1,2-anhydro-3,4-di-O-benzyl-5-benzyloxymethylcyclohexan-1,2,3,4-tetraol

Base Information

Chemical Name:(1R,2R,3S,4R,5R)-1,2-anhydro-3,4-di-O-benzyl-5-benzyloxymethylcyclohexan-1,2,3,4-tetraol
CAS No.:152203-03-7
Molecular Formula:C₂₈H₃₀O₄
Molecular Weight:430.544
Hs Code.:

Synonyms:(1R,2R,3S,4R,5R)-1,2-anhydro-3,4-di-O-benzyl-5-benzyloxymethylcyclohexan-1,2,3,4-tetraol

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Chemical Property of (1R,2R,3S,4R,5R)-1,2-anhydro-3,4-di-O-benzyl-5-benzyloxymethylcyclohexan-1,2,3,4-tetraol

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Technology Process of (1R,2R,3S,4R,5R)-1,2-anhydro-3,4-di-O-benzyl-5-benzyloxymethylcyclohexan-1,2,3,4-tetraol

There total 8 articles about (1R,2R,3S,4R,5R)-1,2-anhydro-3,4-di-O-benzyl-5-benzyloxymethylcyclohexan-1,2,3,4-tetraol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 158182-10-6
(1R,2R,3R,4S,6R)-1,2-di-O-benzyl-6-benzyloxymethyl-4-iodocyclohexane-1,2,3-triol

: 152203-03-7
(1R,2R,3S,4R,5R)-1,2-anhydro-3,4-di-O-benzyl-5-benzyloxymethylcyclohexan-1,2,3,4-tetraol

Guidance literature:: With sodium methylate; In methanol; for 0.0833333h; Ambient temperature;
DOI:10.1016/0957-4166(94)80177-0

Reference yield: 73.0%

: 6-O-benzyl-1,2-anhydro-5α-carba-β-D-mannopyranose

: 100-39-0
benzyl bromide

: 152203-03-7
(1R,2R,3S,4R,5R)-1,2-anhydro-3,4-di-O-benzyl-5-benzyloxymethylcyclohexan-1,2,3,4-tetraol

Guidance literature:: 6-O-benzyl-1,2-anhydro-5α-carba-β-D-mannopyranose; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 0.5h;

benzyl bromide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;
DOI:10.1039/c6ra20401e

Reference yield: 68.0%

: 158250-56-7
(3R,4R,5R)-3,4-dibenzyloxy-5-(benzyloxymethyl)cyclohexene

: 152203-03-7
(1R,2R,3S,4R,5R)-1,2-anhydro-3,4-di-O-benzyl-5-benzyloxymethylcyclohexan-1,2,3,4-tetraol

: (1S,2S,3S,4R,5R)-1,2-anhydro-3,4-di-O-benzyl-5-benzyloxymethylcyclohexan-1,2,3,4-tetraol

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1016/0957-4166(94)80177-0