(5S,6R)-6-{3-[(tert-butyldiphenyl)oxy]propyl}-5-methyltetrahydro-2H-pyran-2-one

Base Information

Chemical Name:(5S,6R)-6-{3-[(tert-butyldiphenyl)oxy]propyl}-5-methyltetrahydro-2H-pyran-2-one
CAS No.:1340479-62-0
Molecular Formula:C₂₅H₃₄O₃Si
Molecular Weight:410.629
Hs Code.:

Synonyms:(5S,6R)-6-{3-[(tert-butyldiphenyl)oxy]propyl}-5-methyltetrahydro-2H-pyran-2-one

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Chemical Property of (5S,6R)-6-{3-[(tert-butyldiphenyl)oxy]propyl}-5-methyltetrahydro-2H-pyran-2-one

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Technology Process of (5S,6R)-6-{3-[(tert-butyldiphenyl)oxy]propyl}-5-methyltetrahydro-2H-pyran-2-one

There total 6 articles about (5S,6R)-6-{3-[(tert-butyldiphenyl)oxy]propyl}-5-methyltetrahydro-2H-pyran-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₃₄O₄Si

: 1340479-62-0
(5S,6R)-6-{3-[(tert-butyldiphenyl)oxy]propyl}-5-methyltetrahydro-2H-pyran-2-one

Guidance literature:: With camphor-10-sulfonic acid; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/ol202483u

Reference yield:

: 1269618-58-7
(3S,4R)-7-[(tert-butyldiphenyl)oxy]-3-methyl-hept-1-en-4-ol

: 1340479-62-0
(5S,6R)-6-{3-[(tert-butyldiphenyl)oxy]propyl}-5-methyltetrahydro-2H-pyran-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 2 h / 80 °C / Inert atmosphere; Microwave irradiation

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 2 h / 20 °C

3: camphor-10-sulfonic acid / dichloromethane / 2 h / 20 °C

With Hoveyda-Grubbs catalyst second generation; palladium 10% on activated carbon; camphor-10-sulfonic acid; hydrogen; In dichloromethane; ethyl acetate;
DOI:10.1021/ol202483u

Reference yield:

: 1340479-61-9
methyl (2E,4S,5R)-5-hydroxy-8-[(tert-butyldiphenyl)oxy]-4-methyl-oct-2-enoate

: 1340479-62-0
(5S,6R)-6-{3-[(tert-butyldiphenyl)oxy]propyl}-5-methyltetrahydro-2H-pyran-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 2 h / 20 °C

2: camphor-10-sulfonic acid / dichloromethane / 2 h / 20 °C

With palladium 10% on activated carbon; camphor-10-sulfonic acid; hydrogen; In dichloromethane; ethyl acetate;
DOI:10.1021/ol202483u