2,4-bis<1-acetyl-4,5-dihydro-(4-methoxyphenyl)pyrazol-3-yl>phenoxyacetic acid hydrazide

Base Information

Chemical Name:2,4-bis<1-acetyl-4,5-dihydro-(4-methoxyphenyl)pyrazol-3-yl>phenoxyacetic acid hydrazide
CAS No.:106924-31-6
Molecular Formula:C₃₂H₃₄N₆O₆
Molecular Weight:598.659
Hs Code.:

Synonyms:2,4-bis<1-acetyl-4,5-dihydro-(4-methoxyphenyl)pyrazol-3-yl>phenoxyacetic acid hydrazide

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Chemical Property of 2,4-bis<1-acetyl-4,5-dihydro-(4-methoxyphenyl)pyrazol-3-yl>phenoxyacetic acid hydrazide

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Technology Process of 2,4-bis<1-acetyl-4,5-dihydro-(4-methoxyphenyl)pyrazol-3-yl>phenoxyacetic acid hydrazide

There total 7 articles about 2,4-bis<1-acetyl-4,5-dihydro-(4-methoxyphenyl)pyrazol-3-yl>phenoxyacetic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 106924-28-1
ethyl 2,4-bis<1-acetyl-4,5-dihydro-5-(4-methoxyphenyl)pyrazol-3-yl>phenoxyacetate

: 106924-31-6
2,4-bis<1-acetyl-4,5-dihydro-(4-methoxyphenyl)pyrazol-3-yl>phenoxyacetic acid hydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 10h; Heating;

Reference yield:

: 30186-16-4
2,4-diacetylphenol

: 106924-31-6
2,4-bis<1-acetyl-4,5-dihydro-(4-methoxyphenyl)pyrazol-3-yl>phenoxyacetic acid hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / potassium hydroxide / methanol / 48 h / 25 °C

2: 91 percent / hydrazine hydrate / 6 h / Heating

3: 78 percent / potassium carbonate / dimethylformamide

4: 82 percent / hydrazine hydrate / ethanol / 10 h / Heating

With potassium hydroxide; potassium carbonate; hydrazine hydrate; In methanol; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 13031-43-1
4-acetyloxyacetophenone

: 106924-31-6
2,4-bis<1-acetyl-4,5-dihydro-(4-methoxyphenyl)pyrazol-3-yl>phenoxyacetic acid hydrazide

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / aluminium chloride / 3 h / 150 °C

2: 85 percent / potassium hydroxide / methanol / 48 h / 25 °C

3: 91 percent / hydrazine hydrate / 6 h / Heating

4: 78 percent / potassium carbonate / dimethylformamide

5: 82 percent / hydrazine hydrate / ethanol / 10 h / Heating

With potassium hydroxide; aluminium trichloride; potassium carbonate; hydrazine hydrate; In methanol; ethanol; N,N-dimethyl-formamide;