(E)-3-cyclohexyl-N,N-diethylacrylamide

Base Information

Chemical Name:(E)-3-cyclohexyl-N,N-diethylacrylamide
CAS No.:948916-65-2
Molecular Formula:C₁₃H₂₃NO
Molecular Weight:209.332
Hs Code.:

Synonyms:(E)-3-cyclohexyl-N,N-diethylacrylamide

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Chemical Property of (E)-3-cyclohexyl-N,N-diethylacrylamide

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Technology Process of (E)-3-cyclohexyl-N,N-diethylacrylamide

There total 4 articles about (E)-3-cyclohexyl-N,N-diethylacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 921-88-0
N,N-diethyldichloroacetamide

: 2043-61-0
cyclohexanecarbaldehyde

: 948916-65-2
(E)-3-cyclohexyl-N,N-diethylacrylamide

Guidance literature:: With 2-phenylpyridine; manganese chloride bis(lithium chloride); lithium; In tetrahydrofuran; for 5h; Heating;
DOI:10.1021/jo701417z

Reference yield:

: 395059-78-6
2-chloro-3-cyclohexyl-N,N-diethyl-3-hydroxypropanamide

: 948916-65-2
(E)-3-cyclohexyl-N,N-diethylacrylamide

Guidance literature:: With samarium diiodide; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1002/1521-3765(20011001)7:19<4266::AID-CHEM4266>3.0.CO;2-8

Reference yield:

: 2315-36-8
2-Chloro-N,N-diethylacetamide

: 948916-65-2
(E)-3-cyclohexyl-N,N-diethylacrylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: LDA / tetrahydrofuran; diethyl ether / 0.17 h / -85 °C

1.2: tetrahydrofuran; diethyl ether / 1 h / -78 °C

2.1: SmI₂ / tetrahydrofuran / 2 h / 20 °C

With samarium diiodide; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;
DOI:10.1002/1521-3765(20011001)7:19<4266::AID-CHEM4266>3.0.CO;2-8