Technology Process of C15H10Br2FNO
There total 5 articles about C15H10Br2FNO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium phosphate;
copper(l) iodide; N,N`-dimethylethylenediamine;
In
1,4-dioxane;
for 48h;
Reflux;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: bromine; acetic acid / 1 h / 0 °C
2.1: potassium carbonate / acetone / 18 h / 20 °C
3.1: N,N-dimethyl-formamide / 3 h / Reflux; Inert atmosphere
4.1: zinc; acetic acid / 0.5 h / Reflux
4.2: 20 °C
5.1: potassium phosphate / copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 48 h / Reflux; Inert atmosphere
With
potassium phosphate; bromine; potassium carbonate; acetic acid; zinc;
copper(l) iodide; N,N`-dimethylethylenediamine;
In
1,4-dioxane; N,N-dimethyl-formamide; acetone;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: zinc; acetic acid / 0.5 h / Reflux
1.2: 20 °C
2.1: potassium phosphate / copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 48 h / Reflux; Inert atmosphere
With
potassium phosphate; acetic acid; zinc;
copper(l) iodide; N,N`-dimethylethylenediamine;
In
1,4-dioxane;